1-苯基-2-丙烯-1-醇合成路线 (共 252 条)
反应条件
3-chloro-benzenecarboperoxoic acid in methanol T=25°C; 1 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 471 - 480
反应条件
phosphorous acid trimethyl ester in methanol T=25°C; 48 h;
参考文献
Chemische Berichte, , vol. 113, # 3 p. 831 - 844
反应条件
sodium tetrahydroborate; cerium(III) chloride in methanol 0.0833333 h; Ambient temperature;
参考文献
Tetrahedron: Asymmetry, , vol. 5, # 1 p. 23 - 26
反应条件
sodium hydroxide; tellurium; adogen 464; hydroxymethanesulfinic acid sodium salt in water; toluene 2 h;
参考文献
Tetrahedron, , vol. 53, # 36 p. 12131 - 12146
反应条件
(C4H9)2(tert-C4H9)SnCl; sodium cyanoborohydride in tert-butyl alcohol T=33°C; 16 h; Ultrasound with 20 KHz and bubbling of air;
参考文献
Chemistry Letters, , # 8 p. 705 - 706
反应条件
potassium carbonate; 3,4,5-trimethoxyphenylboronic acid; [Ru(cyclopentadienyl)(MeCN)3]PF6 in acetonitrile T=90°C; 16 h;
参考文献
New Journal of Chemistry, , vol. 32, # 6 p. 929 - 931
反应条件
chromium dichloride; niobium bromide in N,N-dimethyl-formamide Ambient temperatureelectrolysis: undivided cell, Al anode, Pt cathode, 2 V, 20-10 mA, 5.9 F/mol; Title compound not separated from byproducts;
参考文献
Synlett, , # 1 p. 69 - 70
反应条件
1: 85 percent / potassium carbonate / NaI / acetone / 5 h / Heating 2: 18 percent / t-BuLi / tetrahydrofuran; pentane / 3 h / -78 - 0 °C View Scheme
参考文献
Organic Letters, , vol. 4, # 9 p. 1587 - 1590
反应条件
1.1: 70 percent / PBu3 / tetrahydrofuran 2.1: 4 Angstroem molecular sieves; cumene hydroperoxide / VO(acac)2 / CH2Cl2 / 0.5 h / -10 °C 3.1: 4 Angstroem molecular sieves; VO(acac)2 / CH2Cl2 3.2: cumene hydrogen peroxide / -10 °C 3.3: 70 percent / PBu3 / -10 °C View Scheme
参考文献
Chemical Communications, , # 20 p. 2031 - 2032
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane
参考文献
Journal of the American Chemical Society, , vol. 96, p. 2576 - 2580