1-苯基-2-丙烯-1-醇合成路线 (共 252 条)
反应条件
in tetrahydrofuran Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 52, # 16 p. 3524 - 3528
反应条件
Echerichia coli JM 109(pTAB19) in phosphate buffer; 2,2,4-trimethylpentane T=30°C; Epoxidation; pH=7; Microbiological reaction;
参考文献
Tetrahedron Letters, , vol. 41, # 47 p. 9157 - 9161
反应条件
1.1: ozone / dichloromethane / -78 °C 1.2: -78 - 20 °C / Inert atmosphere 1.3: 20 °C / Inert atmosphere 2.1: tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 22 p. 6018 - 6021
反应条件
1.1: (SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium / dichloromethane / 80 °C / Inert atmosphere; Microwave irradiation 1.2: 2 h / 20 °C / Inert atmosphere; Microwave irradiation 2.1: iron(III) chloride hexahydrate / dichloromethane; water / 4.5 h / 20 °C / Inert atmosphere 3.1: ozone / dichloromethane / -78 °C 3.2: -78 - 20 °C / Inert atmosphere 3.3: 20 °C / Inert atmosphere 4.1: tetrahydrofuran / 2.5 h / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 22 p. 6018 - 6021
参考文献
Tetrahedron: Asymmetry, , vol. 3, # 11 p. 1369 - 1372
反应条件
oxygen; tri-n-butyl-tin hydride in toluene T=15 - 20°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 113, # 23 p. 8980 - 8982
反应条件
N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate in water T=70°C; 3 h;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 47, # 1 p. 290 - 295
反应条件
1: 97 percent / Na2EDTA; di(chloromethyl)dioxirane; Bu4NHSO4 / acetonitrile 2: 41 percent / tBuOK / tetrahydrofuran / -78 °C View Scheme
参考文献
Heteroatom Chemistry, , vol. 13, # 4 p. 310 - 315
反应条件
1: 84 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature 2: 100 percent / Mg / methanol / 2 h / -23 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 6 p. 1523 - 1530
反应条件
(i) Mg, BrCH2CH2Br, Et2O, (ii) /BRN= 741856/; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 90, p. 1619 - 1624