1-苯基-2-丙烯-1-醇合成路线 (共 252 条)
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 12 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 1179 - 1184
反应条件
air T=15 - 20°C; 24 h; var. oxidants or instead of oxidants: air. Var. time.; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 26, # 7 p. 921 - 924
反应条件
in ethanol T=25°C; 20 h;
参考文献
Tetrahedron Letters, , vol. 36, # 37 p. 6725 - 6728
反应条件
1: 2.) Et3N; 3.) Bu3SnH / 1.) MeCN, r.t. 2: 70 percent / tBuOOLi / -78 - 0 °C 3: 39 percent / lithium t-butoxide / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 17 p. 3055 - 3058
反应条件
1: 70 percent / tBuOOLi / -78 - 0 °C 2: 39 percent / lithium t-butoxide / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 17 p. 3055 - 3058
反应条件
caesium carbonate in water T=25°C; 12 h; shaking; optical yield given as percent de;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 21 p. 4876 - 4878
反应条件
MoO(O2)(3,5-dimethylpyrazole)2; dihydrogen peroxide; oxygen in acetonitrile 8 h; Heatingatmospheric pressure;
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4915 - 4917
反应条件
1: 73 percent / Pd(DBA)2 / tetrahydrofuran / 12 h / 20 °C 2: 97 percent / Na2EDTA; di(chloromethyl)dioxirane; Bu4NHSO4 / acetonitrile 3: 41 percent / tBuOK / tetrahydrofuran / -78 °C View Scheme
参考文献
Heteroatom Chemistry, , vol. 13, # 4 p. 310 - 315
反应条件
1: CBr4, PPh3 2: 95 percent / sonicated zinc dust and copper(I) iodide / aq. ethanol / sonication; other 2,3-epoxyalkylhalides View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 818 - 820
反应条件
potassium acetate T=90 - 100°C; Behandlung des Reaktionsprodukts mit wss.-aethanol. NaOH;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 508, p. 58
Journal of the Chemical Society, , p. 1266
Journal of the Chemical Society, , p. 507,510