1-苯基-2-丙烯-1-醇合成路线 （共 252 条）
反应条件
in tetrahydrofuran; diethyl ether T=0°C; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 31 p. 5587 - 5590
反应条件
1: 1.) lithium diisopropylamide / 1.) THF, 15 min, -78 deg C, 2.) 30 min, THF 2: 87 percent / CH2Cl2 3: 74 percent / lithium diisopropylamide / tetrahydrofuran / 0.17 h / -40 °C 4: 58 percent / trimethyl phosphite / methanol / 48 h / 25 °C View Scheme
参考文献
Chemische Berichte, , vol. 113, # 3 p. 831 - 844
反应条件
1: 87 percent / CH2Cl2 2: 74 percent / lithium diisopropylamide / tetrahydrofuran / 0.17 h / -40 °C 3: 58 percent / trimethyl phosphite / methanol / 48 h / 25 °C View Scheme
参考文献
Chemische Berichte, , vol. 113, # 3 p. 831 - 844
反应条件
1: 74 percent / lithium diisopropylamide / tetrahydrofuran / 0.17 h / -40 °C 2: 58 percent / trimethyl phosphite / methanol / 48 h / 25 °C View Scheme
参考文献
Chemische Berichte, , vol. 113, # 3 p. 831 - 844
反应条件
1: 51 percent / m-chloroperbenzoic acid / CH2Cl2 / 3 h / Ambient temperature 2: 92 percent / LDA / diethyl ether; tetrahydrofuran / 24 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 1179 - 1184
反应条件
oxygen; 2,5,7,8-tetramethyl-2-(4',8',12'-trimethyltridecyl)-6-chromanol in benzene T=37°C; 4 h; Kinetics;
参考文献
Chemical Communications, , # 10 p. 1252 - 1254
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in tetrahydrofuran
参考文献
Journal of the Chemical Society, Chemical Communications, , # 18 p. 1419 - 1420
反应条件
oxygen; 2,5,7,8-tetramethyl-2-(4',8',12'-trimethyltridecyl)-6-chromanol in benzene T=25°C; 0.5 h; Irradiation; Kinetics; Further Variations:SolventsReagents;
参考文献
Chemical Communications, , # 10 p. 1252 - 1254
反应条件
indium; oxygen 1.) DMF, 1 h, RT, 2.) room temperature, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 7 p. 2538 - 2542
反应条件
in tetrahydrofuran 1.) -10 deg C to 0 deg C, 30 min, 2.) r.t., 2 h;
参考文献
Tetrahedron Letters, , vol. 35, # 13 p. 2009 - 2012
