3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
in dichloromethane 1.) 0 deg C, 2.) room temperature, 1 h; Yield given;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Verardo, Giancarlo
Tetrahedron, 1994 , vol. 50, # 1 p. 217 - 254
参考文献
Milas; Sussman; Mason
Journal of the American Chemical Society, 1939 , vol. 61, p. 1845
Full Text Show Details
Research Corp. New York
Patent: US2414385 , 1942 ;
反应条件
beim Ozonisieren und Behandeln des Ozonids mit Zinkstaub;
参考文献
Fischer,H. O. L.; Feldmann
Chemische Berichte, 1929 , vol. 62, p. 857
Full Text Show Details
Fischer,H. O. L.; Taube
Chemische Berichte, 1927 , vol. 60, p. 1707
反应条件
camphor-10-sulfonic acid in dichloromethane T=20°C; 24 h;
参考文献
Stewart, Catherine A.; Peng, Xiaowen; Paquette, Leo A.
Synthesis, 2008 , # 3 p. 433 - 437
反应条件
magnesium oxide in various solvent(s) T=0 - 20°C;
参考文献
Nwoye, Ernest O.; Dudley, Gregory B.
Chemical Communications, 2007 , # 14 p. 1436 - 1437
反应条件
1: 87 percent / (+)-diisopropyl tartrate, Ti(OiPr)4, tBuOOH 2: 1) NaIO4, RuCl3 / 1) MeCN, CCl4, H2O 3: 98 percent / MgBr2*Et2O / diethyl ether / 1) -60 deg C, 2 h, 2) -40 deg C, 4 h 4: 98 percent / NaN3 / acetone; H2O 5: 96 percent / DMAP, Et3N 6: 88 percent / H2 / Pd/C / methanol View Scheme
参考文献
Bonini; Righi
Journal of the Chemical Society - Series Chemical Communications, 1994 , # 24 p. 2767 - 2768
参考文献
Staiger; Miller
Journal of Organic Chemistry, 1959 , vol. 24, p. 1214,1216, 1218
反应条件
1: 3-chloro-benzenecarboperoxoic acid 2: chloro-trimethyl-silane / ethyl acetate / -20 °C 3: isopropyl alcohol 4: hydrogenchloride / water; ethyl acetate 5: sodium hydroxide / toluene 6: methanol; ammonia / isopropyl alcohol 7: carbonic acid dimethyl ester / ethanol 8: potassium tert-butylate / isopropyl alcohol; tert-butyl alcohol 9: methanesulfonic acid / acetone View Scheme
参考文献
Assaf, Georges; Checksfield, Graham; Critcher, Doug; Dunn, Peter J.; Field, Stuart; Harris, Laurence J.; Howard, Roger M.; Scotney, Gemma; Scott, Adam; Mathew, Suju; Walker, Geoffrey M. H.; Wilder, Alexander
Green Chemistry, 2012 , vol. 14, # 1 p. 123 - 129
反应条件
1: triethylamine / diethyl ether / 18 h / Ambient temperature 2: <Rh((S,S)-chiraphos)>2(ClO4)2 / acetone / 0.3 h / 25 °C 3: KF, KHCO3, 30percent aq. H2O2 / methanol; tetrahydrofuran / 18 h / Heating View Scheme
参考文献
Cui, Yong-Mei; Huang, Qing-Qing; Xu, Jie; Chen, Ling-Ling; Li, Jing-Ya; Ye, Qi-Zhuang; Li, Jia; Nan, Fa-Jun
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 18 p. 4130 - 4135
反应条件
[Cp*Ir(SnCl3)2{SnCl2(H2O)2}] in dichloromethane T=20°C; Inert atmosphereSchlenk technique; regioselective reaction;
参考文献
Maity, Arnab Kumar; Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2013 , vol. 69, # 2 p. 942 - 956
