3-苯基丙-2-烯-1-醇合成路线 (共 318 条)
反应条件
(i) SOCl2, Py, benzene, (ii) /BRN= 741973/; Multistep reaction;
参考文献
Hu, Li Hong; Zou, Hong Bin; Gong, Jing Xu; Li, Hai Bo; Yang, Lei Xiang; Cheng, Wei; Zhou, Chang Xin; Bai, Hua; Gueritte, Francoise; Zhao, Yu
Journal of Natural Products, 2005 , vol. 68, # 3 p. 342 - 348
反应条件
amberlyst-15; 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=110°C; 0.666667 h; microwave irradiation;
参考文献
Sinha, Arun K.; Sharma, Anuj; Swaroop, Anand; Kumar, Vinod
Tetrahedron, 2007 , vol. 63, # 4 p. 1000 - 1007
反应条件
4-Methylpyridine in dichloromethane 1 h; Reflux;
参考文献
Chantarasriwong, Oraphin; Jang, Doo Ok; Chavasiri, Warinthorn
Synthetic Communications, 2008 , vol. 38, # 16 p. 2845 - 2856
反应条件
osmium(VIII) oxide in water; tert-butyl alcohol T=20°C; 19 h; Inert atmosphere;
参考文献
Synthesis (Germany), , vol. 45, # 20 art. no. SS-2013-T0380-OP, p. 2875 - 2887
反应条件
tetrapropylammonium perruthennate in dichloromethane 0.5 h; Molecular sieveInert atmosphere;
参考文献
Koerber, Jochen; Loeffler, Stefan; Schollmeyer, Dieter; Nubbemeyer, Udo
Synthesis (Germany), 2013 , vol. 45, # 20 art. no. SS-2013-T0380-OP, p. 2875 - 2887
反应条件
tetrapropylammonium perruthennate in dichloromethane 0.5 h; Molecular sieveInert atmosphere;
参考文献
Koerber, Jochen; Loeffler, Stefan; Schollmeyer, Dieter; Nubbemeyer, Udo
Synthesis (Germany), 2013 , vol. 45, # 20 art. no. SS-2013-T0380-OP, p. 2875 - 2887
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trifluoroacetic acid in toluene T=105°C; P=30003 Torr; 22 h; Inert atmosphereAutoclave; regioselective reaction;
参考文献
Liu, Qiang; Wu, Lipeng; Jiao, Haijun; Fang, Xianjie; Jackstell, Ralf; Beller, Matthias
Angewandte Chemie - International Edition, 2013 , vol. 52, # 31 p. 8064 - 8068
Angew. Chem., 2013 , vol. 125, # 31 p. 8222 - 8226,5
反应条件
triphenylphosphine; bis(η3-allyl-μ-chloropalladium(II)) in water T=110°C; 4 h; Title compound not separated from byproducts;
参考文献
Manabe, Kei; Nakada, Kenji; Aoyama, Naohiro; Kobayashi, Shu
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 11-13 p. 1499 - 1503
反应条件
boric acid in dichloromethane 8 h; RefluxInert atmosphere; regioselective reaction;
参考文献
Tao, Yinsong; Zhou, Yuhan; Qu, Jingping; Hidai, Masanobu
Tetrahedron Letters, 2010 , vol. 51, # 15 p. 1982 - 1984
参考文献
MyCell Holdings Limited
Patent: US2011/130562 A1, 2011 ;