3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
Multistep reaction.;
参考文献
Nakashima, Katsuyuki; Kikuchi, Naoki; Shirayama, Daisuke; Miki, Takuo; Ando, Kazuhiro; Sono, Masakazu; Suzuki, Shinya; Kawase, Masaki; Kondoh, Masuo; Sato, Masao; Tori, Motoo
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 2 p. 387 - 394
参考文献
Benoit; Herzog
Bulletin des Sciences Pharmacologiques, 1935 , vol. 42, p. 102,105
反应条件
tetrakis(triphenylphosphine) palladium(0); carbon dioxide in 1,4-dioxane T=110°C; P=38000 Torr; 40 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 69, # 4 p. 1065 - 1078
反应条件
1.1: toluene-4-sulfonic acid; [Pd(C,N-C6H4CH2NMe2)Cl]2 / methanol; dimethyl sulfoxide / 50 °C / |Inert atmosphere 2.1: potassium tert-butylate; [Cu(N,N′-bis(2,6-diisopropylphenyl)-imidazol-2-ylidene)Cl] / tetrahydrofuran / 16 h / 70 °C / |Inert atmosphere; |Sealed tube 2.2: |Inert atmosphere; |Sealed tube View Scheme
参考文献
Organic Letters, , vol. 15, # 15 p. 4034 - 4037
反应条件
NH4BF4; [(Cp*)RuCl(SMe)]2 in 1,2-dichloro-ethane T=60°C; 1 h;
参考文献
Nishibayashi, Yoshiaki; Milton, Marilyn Daisy; Inada, Youichi; Yoshikawa, Masato; Wakiji, Issei; Hidai, Masanobu; Uemura, Sakae
Chemistry - A European Journal, 2005 , vol. 11, # 5 p. 1433 - 1451
反应条件
sulfuric acid stereoisomer(ic) of mp: 260 degree;
参考文献
Braude; Forbes
Journal of the Chemical Society, 1951 , p. 1755,1760
反应条件
1: 1) NaH / 1) THF, 2) room temperature, 1 h 2: 50 percent / BCl3 / pentane; hexane / 1 h / Ambient temperature 3: 45 percent / tetrahydrofuran; dimethylformamide View Scheme
参考文献
Bedford; Harris III; Howd; Goff; Koolpe; Petesch; Koplovitz; Sultan; Musallam
Journal of Medicinal Chemistry, 1989 , vol. 32, # 2 p. 504 - 516
反应条件
tert.-butylhydroperoxide; copper(l) chloride in decane; acetonitrile T=20°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 49, # 15 p. 2457 - 2460
反应条件
dihydrogen peroxide; Manganese (II) acetate in water T=25°C; Ionic liquid; chemoselective reaction;
参考文献
Applied Catalysis A: General, , vol. 453, p. 244 - 249
反应条件
sodium hydroxide; dipotassium peroxodisulfate; nickel sulphate in dichloromethane; water 6 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1361 - 1364
