3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
反应条件
1.1: (+)-diethyl tartrate; Ti(O-i-Pr)4; tert-butylhydroperoxide
1.2: triethylamine; 4-(dimethylamino)pyridine
1.3: p-toluenesulfonic acid / tetrahydrofuran; H2O
2.1: p-toluenesulfonic acid / acetone / 20 °C
3.1: tetrabutylammonium fluoride / tetrahydrofuran / 20 °C
View Scheme
参考文献
Yang; Zhou
Journal of the Chemical Society - Series Chemical Communications, 1995 , # 7 p. 743 - 744
反应条件
Multistep reaction.;
参考文献
Nakashima, Katsuyuki; Kikuchi, Naoki; Shirayama, Daisuke; Miki, Takuo; Ando, Kazuhiro; Sono, Masakazu; Suzuki, Shinya; Kawase, Masaki; Kondoh, Masuo; Sato, Masao; Tori, Motoo
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 2 p. 387 - 394
反应条件
1-chloro-2-methyl-N,N-tetramethylenepropenylamine in tetrahydrofuran; dichloromethane
T=-30 - 0°C; 0.75 h; Yield given. Yields of byproduct given;
参考文献
Fujisawa, Tamotsu; Iida, Sachio; Yukizaki, Hisashi; Sato, Toshio
Tetrahedron Letters, 1983 , vol. 24, # 51 p. 5745 - 5748
反应条件
hexamethyltriamido-N-benzylimidophosphate in tetrahydrofuran
T=20°C; Acylation; 17 h;
参考文献
Ilankumaran, Palanichamy; Verkade, John G.
Journal of Organic Chemistry, 1999 , vol. 64, # 25 p. 9063 - 9066
反应条件
cobalt(II) chloride
T=80°C; 8 h;
参考文献
Bosco, J. W. John; Raju, B. Rama; Saikia, Anil K.
Synthetic Communications, 2004 , vol. 34, # 15 p. 2849 - 2855
反应条件
trimethylsilyl trifluoromethanesulfonate in ethyl acetate
T=-10°C; 10 h;
参考文献
Chakraborti, Asit K.; Sharma, Lalima; Gulhane, Rajesh; Shivani
Tetrahedron, 2003 , vol. 59, # 39 p. 7661 - 7668
反应条件
N,N'-biscyclohexyl-imidazol-2-ylidene; 5A molecular sieve in tetrahydrofuran
T=20°C; 1 h;
参考文献
Grasa, Gabriela A.; Kissling, Rebecca M.; Nolan, Steven P.
Organic Letters, 2002 , vol. 4, # 21 p. 3583 - 3586
反应条件
tributyl-amine; acetic acid in dichloromethane
参考文献
Sumitomo Chemical Company, Limited
Patent: US4206310 A1, 1980 ;
反应条件
N,N'-bismesityl-imidazol-2-ylidene in tetrahydrofuran
T=20°C; 3 h;
参考文献
Grasa, Gabriela A.; Gueveli, Tatyana; Singh, Rohit; Nolan, Steven P.
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2812 - 2819
反应条件
aluminum oxide
T=25°C; 0.166667 h;
参考文献
Yadav, Veejendra K.; Babu, K. Ganesh
Journal of Organic Chemistry, 2004 , vol. 69, # 2 p. 577 - 580
