3-苯基丙-2-烯-1-醇合成路线 (共 318 条)
反应条件
cobalt(II) chloride in acetonitrile
T=25°C; 4 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
[(nBuSn)12(μ3-O)14(μ2-OH)6](2+)*2(2,5-Me2C6H3SO3(1-))
T=75°C; 4.5 h;
参考文献
Chandrasekhar, Vadapalli; Boomishankar, Ramamoorthy; Gopal, Kandasamy; Sasikumar, Palani; Singh, Puja; Steiner, Alexander; Zacchini, Stefano
European Journal of Inorganic Chemistry, 2006 , # 20 p. 4129 - 4136
反应条件
acetyl chloride in dichloromethane
1.) 0 deg C, 2.) room temperature, 1 h; Yields of byproduct given;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Verardo, Giancarlo
Tetrahedron, 1994 , vol. 50, # 1 p. 217 - 254
反应条件
anhydrous lithium nitrate; scandium tris(trifluoromethanesulfonate) in acetonitrile
T=20°C; 4 h;
参考文献
Kawada, Atsushi; Takeda, Shigemitsu; Yamashita, Kazumi; Abe, Hitoshi; Harayama, Takashi
Chemical and Pharmaceutical Bulletin, 2002 , vol. 50, # 8 p. 1060 - 1065
反应条件
in acetonitrile
16 h; UV-irradiation;
参考文献
Debieux, Jean-Luc; Cosandey, Anne; Helgen, Celine; Bochet, Christian G.
European Journal of Organic Chemistry, 2007 , # 13 p. 2073 - 2077
反应条件
sodium acetate; acetic acid
参考文献
Tseou; Wang
Journal of the Chinese Chemical Society (Peking), 1937 , vol. 5, p. 224
Chem. Zentralbl., 1937 , vol. 108, # II p. 3310
反应条件
in dichloromethane
1.) 0 deg C, 2.) room temperature, 1 h; Yield given;
参考文献
Strazzolini, Paolo; Giumanini, Angelo G.; Verardo, Giancarlo
Tetrahedron, 1994 , vol. 50, # 1 p. 217 - 254
反应条件
silica gel
T=20°C; 12 h;
参考文献
Sampath Kumar; Joyasawal, Sipak; Reddy; Pawan Chakravarthy; Krishna; Yadav
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 8 p. 1686 - 1692
反应条件
Montmorillonite KSF
T=100°C; Claisen-Johnson orthoester rearrangement; 6 h; Further byproducts given;
参考文献
Sampath Kumar; Joyasawal, Sipak; Reddy; Pawan Chakravarthy; Krishna; Yadav
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 8 p. 1686 - 1692
反应条件
n-butyllithium; [Rh(dppe)(NBD)]ClO4
1.) THF, hexane, reflux, 8 h, 2.) THF, hexane; Yield givenMultistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gazzard, Lewis J.; Motherwell, William B.; Sandham, David A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 979 - 993