3-[5-(3-羟基丙基)-2-呋喃]-丙烷-1-醇合成路线 （共 12 条）
反应条件
1: With oxygen; methylene blue in dichloromethane T=0°C; 0.0333333 h; Irradiation; 2: With dimethylsulfide in dichloromethane T=20°C;
参考文献
Georgiou, Thomas; Tofi, Maria; Montagnon, Tamsyn; Vassilikogiannakis, Georgios
Organic Letters, 2006 , vol. 8, # 9 p. 1945 - 1948
反应条件
1: With sodium tetrahydroborate; lithium chloride in tetrahydrofuran; ethanol
T=20°C; 12 h;
2: With hydrogen; palladium on activated charcoal in ethanol
参考文献
McDermott, Paul J.; Stockman, Robert A.
Organic Letters, 2005 , vol. 7, # 1 p. 27 - 29
反应条件
lithium aluminium tetrahydride in diethyl ether
T=0 - 20°C;
参考文献
Georgiou, Thomas; Tofi, Maria; Montagnon, Tamsyn; Vassilikogiannakis, Georgios
Organic Letters, 2006 , vol. 8, # 9 p. 1945 - 1948
反应条件
copper oxide-chromium oxide
T=145 - 175°C; P=147102 Torr; Hydrogenation;
参考文献
Webb; Borcherdt
Journal of the American Chemical Society, 1951 , vol. 73, p. 752
反应条件
lithium aluminium tetrahydride in diethyl ether
12 h; Heating;
参考文献
Cattalini, Marco; Cossu, Sergio; Fabris, Fabrizio; De Lucchi, Ottorino
Synthetic Communications, 1996 , vol. 26, # 4 p. 637 - 647
反应条件
1: hydrogen / Pd/C
2: 82 percent / LiAlH4 / diethyl ether / 0 - 20 °C
View Scheme
参考文献
Georgiou, Thomas; Tofi, Maria; Montagnon, Tamsyn; Vassilikogiannakis, Georgios
Organic Letters, 2006 , vol. 8, # 9 p. 1945 - 1948
反应条件
1: TsOH
2: LDA
3: HCl
4: hydrogen / Pd/C
5: 82 percent / LiAlH4 / diethyl ether / 0 - 20 °C
View Scheme
参考文献
Georgiou, Thomas; Tofi, Maria; Montagnon, Tamsyn; Vassilikogiannakis, Georgios
Organic Letters, 2006 , vol. 8, # 9 p. 1945 - 1948
反应条件
1: hydrogen / Pd/C
2: 82 percent / LiAlH4 / diethyl ether / 0 - 20 °C
View Scheme
参考文献
Georgiou, Thomas; Tofi, Maria; Montagnon, Tamsyn; Vassilikogiannakis, Georgios
Organic Letters, 2006 , vol. 8, # 9 p. 1945 - 1948
反应条件
1: LDA
2: HCl
3: hydrogen / Pd/C
4: 82 percent / LiAlH4 / diethyl ether / 0 - 20 °C
View Scheme
参考文献
Georgiou, Thomas; Tofi, Maria; Montagnon, Tamsyn; Vassilikogiannakis, Georgios
Organic Letters, 2006 , vol. 8, # 9 p. 1945 - 1948
反应条件
1: HCl
2: hydrogen / Pd/C
3: 82 percent / LiAlH4 / diethyl ether / 0 - 20 °C
View Scheme
参考文献
Georgiou, Thomas; Tofi, Maria; Montagnon, Tamsyn; Vassilikogiannakis, Georgios
Organic Letters, 2006 , vol. 8, # 9 p. 1945 - 1948
