3-(4-甲基苯基)吡啶合成路线 （共 66 条）
反应条件
sodium carbonate; Pd(PPh3)4 in pyridine; water; toluene
参考文献
Halazy, Serge; Quattropani, Anna; Scheer, Alexander; Schwarz, Mattias; Thomas, Russell; Baxter, Antony
Patent: US2003/212012 A1, 2003 ;
反应条件
potassium permanganate in pyridine; water
参考文献
Halazy, Serge; Quattropani, Anna; Bombrun, Agnes; Schwarz, Mattias; Thomas, Russel; Baxter, Anthony
Patent: US2003/171309 A1, 2003 ;
反应条件
C18H20Cl2N8Pd; caesium carbonate in 1,4-dioxane
T=100°C; Suzuki coupling; 12 h; Inert atmosphere;
参考文献
Xu, Chen; Li, Zhen; Duan, Lu-Meng; Wang, Zhi-Qiang; Fu, Wei-Jun; Hao, Xin-Qi; Song, Mao-Ping
Transition Metal Chemistry, 2012 , vol. 37, # 4 p. 373 - 378
反应条件
K3PO4*7H2O; palladium diacetate in ethylene glycol
T=80°C; Suzuki coupling; 0.25 h;
参考文献
Karimi, Babak; Zamani, Asghar
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 23 p. 4531 - 4536
反应条件
copper(l) iodide; C37H51ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide
T=80°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
反应条件
copper(l) iodide; C37H51ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide
T=20°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
反应条件
copper(l) iodide; C52H67ClFeNPPd; cesium fluoride in N,N-dimethyl-formamide
T=110°C; Stille Cross Coupling; 12 h; Inert atmosphere;
参考文献
Ma, Gaizhi; Leng, Yuting; Wu, Yusheng; Wu, Yangjie
Tetrahedron, 2013 , vol. 69, # 2 p. 902 - 909
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; potassium carbonate; PdI2 in water; isopropyl alcohol
T=80°C; Suzuki reaction; 5 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
反应条件
cis-diisothiocyanato-bis[1,3-bis(2-propenyl)benzimidazolin-2-ylidene]nickel(II) in tetrahydrofuran
T=20°C; Kumada-Corriu coupling; 24 h; Inert atmosphere;
参考文献
Jothibasu, Ramasamy; Huang, Kuo-Wei; Huynh, Han Vinh
Organometallics, 2010 , vol. 29, # 17 p. 3746 - 3752
反应条件
sodium hydroxide; [PdCl2(P(3,4-(18-crown-6)-phenyl)2(C6H5))2]
T=140°C; 1.5 h;
参考文献
Gordillo, Alvaro; De Jesus, Ernesto; Lopez-Mardomingo, Carmen
Organic Letters, 2006 , vol. 8, # 16 p. 3517 - 3520
