反应条件
1.1: palladium on carbon; hydrogen / 760.05 Torr 2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere 2.2: -78 - 20 °C 3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 30 °C / Inert atmosphere View Scheme
参考文献
Hermange, Philippe; Lindhardt, Anders T.; Taaning, Rolf H.; Bjerglund, Klaus; Lupp, Daniel; Skrydstrup, Troels
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 6061 - 6071