in carbon disulfide under N2; to a soln. of Fe complex in CS2 a soln. of SCl2 in CS2 was added; pptd. Cp2TiCl2 filtered off, filtrate was stirred with a little SiO2, filtered, filtrate was evapd., residue was chromd. (SiO2, CH2Cl2/hexane (1/4)); elem. anal.;