反应条件
1: 71 percent / Pb(OAc)4, Cu(OAc)2, pyridine / benzene / 8 h / Heating
2: 80 percent / t-C4H9-OOH, aq. 40percent Triton B, OsO4 / 2-methyl-propan-2-ol / 0 °C
3: 1.) 2-acetoxybenzoyl bromide, CH3COOH; 2.) MeONa / 1.) 100 deg C, 2 h; 2.) CH3OH, room temp., 1.5 h
View Scheme
参考文献
Bhat, K. S.; Joshi, P. L.; Rao, A. S.
Synthesis, 1984 , # 2 p. 142 - 145
