3-(羟甲基)苯硼酸频哪醇酯合成路线 （共 10 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 3 h; 2: With water in tetrahydrofuran T=0°C;
参考文献
US2012/309746 A1, ;
Page/Page column 50 ;
US 20120309746 A1
反应条件
sodium tetrahydroborate T=20°C; 5 h;
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
in toluene 2 h; Dean-StarkRefluxInert atmosphere;
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: magnesium sulfate / methanol / 6 h / 20 °C 2: sodium tetrahydroborate / 5 h / 20 °C View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
1: magnesium sulfate / methanol / 6 h / 20 °C 2: sodium tetrahydroborate / 5 h / 20 °C View Scheme
参考文献
Molecules, , vol. 18, # 10 p. 12346 - 12367
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate in tetrahydrofuran; water 16 h; Inert atmosphereReflux;
参考文献
MERCK SHARP and DOHME CORP.; HAGMANN, William K.; NARGUND, Ravi P.; BLIZZARD, Timothy A.; JOSIEN, Hubert; BIJU, Purakkattle; PLUMMER, Christopher W.; DANG, Qun; LI, Bing; LIN, Linus S.; CUI, Mingxiang; HU, Bin; HAO, Jinlai; CHEN, Zhengxia
Patent: WO2014/19186 A1, 2014 ;
Location in patent: Page/Page column 81 ;
