1,2,4-三苯基-1,4-丁二酮合成路线 （共 63 条）
参考文献
Sprio
Gazzetta Chimica Italiana, 1955 , vol. 85, p. 569,573
Full Text Show Details
Lespagnol et al.
Bulletin de la Societe de Pharmacie de Lille, 1955 , p. 87
反应条件
methanol; Mg3N2 T=0 - 80°C; Paal-Knorr pyrrole synthesis;
参考文献
Veitch, Gemma E.; Bridgwood, Katy L.; Rands-Trevor, Karen; Ley, Steven V.
Synlett, 2008 , # 17 p. 2597 - 2600
参考文献
Angelico; Calvello
Gazzetta Chimica Italiana, 1901 , vol. 31, p. II 7
反应条件
T=150°C; im geschlossenen Rohr;
参考文献
Smith
Journal of the Chemical Society, 1890 , vol. 57, p. 644
Chemische Berichte, 1893 , vol. 26, p. 61
参考文献
Angelico; Calvello
Gazzetta Chimica Italiana, 1901 , vol. 31 II, p. 7
反应条件
1: benzaldehyde With 3,3'-(1,4-phenylenebis(methylene))bis(5-(2-hydroxyethyl)-4-methylthiazol-3-ium) bromide; triethylamine in ethanol
T=20°C; Stetter reaction; 0.166667 h;
2: Benzalacetophenone in ethanol
T=70°C; Stetter reaction; 15 h;
参考文献
Lakshmi Reddy; Praveen Kumar; Satyanarayana; Narender; Subba Reddy
Tetrahedron Letters, 2012 , vol. 53, # 13 p. 1546 - 1549
反应条件
potassium hydroxide; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate in water
T=100°C;
参考文献
Huang; Meng; Venkatraman; Wang; Li
Journal of the American Chemical Society, 2001 , vol. 123, # 30 p. 7451 - 7452
反应条件
1: With ozone in dichloromethane
T=-78°C; Inert atmosphere;
2: With triphenylphosphine in dichloromethane
T=-78 - 20°C; Inert atmosphere;
参考文献
Thompson, Benjamin B.; Montgomery, John
Organic Letters, 2011 , vol. 13, # 13 p. 3289 - 3291
反应条件
air; NAF; rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate
T=100°C; 12 h;
参考文献
Huang; Li
Chemical Communications, 2001 , # 22 p. 2348 - 2349
反应条件
sodium hydroxide; 1,2-diphenyl-2-hydroxyethanone in dimethyl sulfoxide
2 h; Ambient temperature;
参考文献
Robinson, J. Michael; Flynn, Emmette T.; McMahan, Terry L.; Simpson, Sharai L.; Trisler, John C.; Conn, Kenneth Bruce
Journal of Organic Chemistry, 1991 , vol. 56, # 23 p. 6709 - 6712
