1-羟基-4,4-二甲基-3-戊酮合成路线 （共 5 条）
反应条件
1: With camphor-10-sulfonic acid; ethylene glycol
Inert atmosphere;
2: With lithium aluminium tetrahydride in diethyl ether
Inert atmosphere;
3: With silica gel
Acidic conditionsInert atmosphere;
参考文献
O'Neil, Gregory W.; Miller, Michael M.; Carter, Kyle P.
Organic Letters, 2010 , vol. 12, # 22 p. 5350 - 5353
反应条件
sodium azide; iodobenzene dichloride in ethyl acetate
T=0 - 80°C; Curtius Rearrangement; 12 h; Inert atmosphere;
参考文献
He, Tian; Gao, Wen-Chao; Wang, Wei-Kun; Zhang, Chi
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 5 p. 1113 - 1118
反应条件
mercury(II) diacetate; acetic acid
参考文献
Wenus-Danilowa; Danilow
Zhurnal Obshchei Khimii, 1932 , vol. 2, p. 645,652, 653
Chem. Zentralbl., C 1933 II 47
反应条件
1: diethyl ether
2: mercury acetate; acetic acid
View Scheme
参考文献
Wenus-Danilowa; Danilow
Zhurnal Obshchei Khimii, 1932 , vol. 2, p. 645,652, 653
Chem. Zentralbl., C 1933 II 47
参考文献
Wenus-Danilowa; Danilow
Zhurnal Obshchei Khimii, 1932 , vol. 2, p. 645,652, 653
Chem. Zentralbl., C 1933 II 47
