1: 3,4,5-trimethoxyphenylboronic acid With diethylzinc in toluene T=60°C; 12 h; 2: ortho-fluorobenzaldehyde With (S,S)-N-(1-Ph-ethyl)-N-[2-OH-bis(1-naphthyl)methyl]NCH3; DiMPEG polyether in toluene T=-10°C; 15 h;
参考文献
Ji, Jian-Xin; Wu, Jing; Au-Yeung, Terry T.-L.; Yip, Chiu-Wing; Haynes, Richard K.; Chan, Albert S. C.
Journal of Organic Chemistry, 2005 , vol. 70, # 3 p. 1093 - 1095
1: triphenyl boroxine With diethylzinc in toluene T=60°C; 0.5 h; 2: ortho-fluorobenzaldehyde in toluene T=10°C; 0.5 h; Further stages. Title compound not separated from byproducts.;
