2-氯-2-苯基苯乙酮合成路线 （共 108 条）
反应条件
1: 5 percent / manganese(III)acetate, LiCl / acetic acid / 0.67 h / Heating 2: 80 percent / manganese(II)acetate, acetic anhydride / acetic acid / 3 h / Heating View Scheme
参考文献
Yonemura, Hiroshi; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3153 - 3160
反应条件
1: Perkin condensation 2: 5 percent / manganese(III)acetate, LiCl / acetic acid / 0.67 h / Heating 3: 80 percent / manganese(II)acetate, acetic anhydride / acetic acid / 3 h / Heating View Scheme
参考文献
Yonemura, Hiroshi; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3153 - 3160
反应条件
1: 28 percent / potassium tert-butoxide / 48 h / 80 °C 2: 100 percent / BF3*Et2O, H2O / dioxane / 10 h / 70 °C View Scheme
参考文献
Dement'eva, L. P.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 117 - 118
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 138 - 139
反应条件
1: 28 percent / potassium tert-butoxide / 48 h / 80 °C 2: 100 percent / BF3*Et2O, H2O / dioxane / 10 h / 70 °C View Scheme
参考文献
Dement'eva, L. P.; Kostikov, R. R.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 117 - 118
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 138 - 139
反应条件
in diethyl ether T=-60°C;
参考文献
Elkik,E.; Assadi-Far,H.
Bulletin de la Societe Chimique de France, 1970 , p. 991 - 998
反应条件
hydrogenchloride in water
参考文献
Eijk, Peter J. S. S. van; Trompenaars, Willem P.; Reinhoudt, David N.; Harkema, Sybolt
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 2 p. 52 - 62
反应条件
Oxonereg;; quartz; sodium chloride in n-heptane 0.333333 h; Milling; chemoselective reaction;
参考文献
Schmidt, Robert; Stolle, Achim; Ondruschka, Bernd
Green Chemistry, 2012 , vol. 14, # 6 p. 1673 - 1679
反应条件
hydrogenchloride; diethyl ether
参考文献
Curtius; Lang
Journal fuer Praktische Chemie (Leipzig), 1891 , vol. <2> 44, p. 564
反应条件
Fe(CH3CN)6(FeCl4)3 in acetonitrile 0.25 h; Ambient temperatureother iron(III) solvates of nitriles, other temperatures, other times; Product distribution;
参考文献
Kotani, Eiichi; Kobayashi, Shigeki; Adachi, Mayumi; Tsujioka, Toshiyuki; Nakamura, Kouji; Tobinaga, Seisho
Chemical & Pharmaceutical Bulletin, 1989 , vol. 37, # 3 p. 606 - 609
反应条件
lithium diisopropyl amide 1) ether, THF, -100 deg C, 1 h; 2) THF, ether, -100 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Larson, Gerald L.; Prieto, Jose A.; Valle, Luis del
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1405 - 1412
