2,4,6-三苯基吡喃鎓四氟硼酸盐合成路线 （共 49 条）
反应条件
1: 68 percent / HOAc / CH2Cl2 / 0.5 h 2: 40 percent / 1.) 10 M NaOH / 1.) EtOH, MeOH, 0-5 deg C, 18 h, 2.) 180-200 deg C, 1-2 mm Hg, 3-4 h View Scheme
参考文献
Katritzky, Alan R.; Rubio, Olga
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 448 - 454
反应条件
N-ethyl-N,N-diisopropylamine in 1,2-dichloro-benzene Heating;
参考文献
Dimroth,K.; Laubert,G.
Angewandte Chemie, 1969 , vol. 81, p. 392 - 393
参考文献
Breit, Bernhard; Winde, Roland; Mackewitz, Thomas; Paciello, Rocco; Harms, Klaus
Chemistry - A European Journal, 2001 , vol. 7, # 14 p. 3106 - 3121
反应条件
sodium acetate; chlorine in tetrachloromethane; ethanol T=65°C; 2 h;
参考文献
Pchelintseva, N. V.; Chalaya, S. N.; Kharchenko, V. G.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 9.1 p. 1603 - 1605
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 9 p. 1854 - 1856
反应条件
in chloroform-d1 Product distributionMechanism;
参考文献
Katritzky, Alan R.; Marquet, Jorge; Lloyd, Jeremy M.; Keay, James G.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 9 p. 1435 - 1442
反应条件
in ethanol
4 h; Ambient temperature;
参考文献
Harris, D. J.; Kan, G. Y.-P.; Tschamber, T.; Snieckus, V.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 494 - 500
反应条件
1: iPr2NEt / chlorobenzene
2: CrO3
View Scheme
参考文献
Dimroth,K.; Laubert,G.
Angewandte Chemie, 1969 , vol. 81, p. 392 - 393
反应条件
in ethanol
T=20°C; 6 h;
参考文献
Katritzky, Alan R.; Thind, Sukhpal S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1895 - 1900
反应条件
in dichloromethane
T=25°C; catalytic effect of acetic acid; Rate constant;
参考文献
Katritzky, Alan R.; Manzo, Ruben H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 571 - 575
反应条件
sodium cyanoborohydride in acetonitrile
T=25°C; Activation energy; Further Variations:Reagents;
参考文献
Heyes, David; Menon, Ramesh S.; Watt; Wiseman, Jake; Kubinski, Przemyslaw
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 10 p. 689 - 700
