Sebacaldehyde合成路线 （共 26 条）
反应条件
TiCl3(DME)2; copper; zinc in ethylene glycol dimethyl ether T=25°C; 38 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
McMurry, John E.; Rico, Joseph G.
Tetrahedron Letters, 1989 , vol. 30, # 10 p. 1169 - 1172
反应条件
potassium permanganate; oxygen
参考文献
v. Braun; Keller
Chemische Berichte, 1933 , vol. 66, p. 219
反应条件
in soda-alkal. Loesung;
参考文献
v. Braun; Keller
Chemische Berichte, 1933 , vol. 66, p. 219
反应条件
hydrogen T=180°C; P=7500.75 - 30003 Torr; 24 h;
参考文献
BASF Aktiengesellschaft
Patent: WO2005/30681 A1, 2005 ;
Location in patent: Page/Page column 74-75 ;
反应条件
potassium hydroxide; PS-resin; potassium hexacyanoferrate(III); 1-oxyl-2,2,6,6-tetramethlpiperidin-4-yl benzoate in water; toluene
T=20°C; 4 h;
参考文献
Yoshitomo, Kashiwagi; Chiba, Shinya; Anzai, Jun-ichi
New Journal of Chemistry, 2003 , vol. 27, # 11 p. 1545 - 1549
反应条件
1: With trimethylsilyl trifluoromethanesulfonate; triphenylphosphine in dichloromethane
T=20°C; 1 h;
2: With diisobutylaluminium hydride in hexane; dichloromethane
T=-78°C; regioselective reaction;
参考文献
Yahata, Kenzo; Minami, Masaki; Yoshikawa, Yuki; Watanabe, Kei; Fujioka, Hiromichi
Chemical and Pharmaceutical Bulletin, 2013 , vol. 61, # 12 p. 1298 - 1307
反应条件
water; [Cp(dppm)RuCl] in isopropyl alcohol
T=100°C; 12 h;
参考文献
Suzuki, Toshiaki; Tokunaga, Makoto; Wakatsuki, Yasuo
Organic Letters, 2001 , vol. 3, # 5 p. 735 - 736
反应条件
thexylbromoborane dimethyl sulfide complex in carbon disulfide; dichloromethane
T=-20 - 20°C; 1 h;
参考文献
Cha, Jin Soon; Kim, Jin Euog; Oh, Se Yeon; Lee, Jae Cheol; Lee, Kwang Woo
Tetrahedron Letters, 1987 , vol. 28, # 21 p. 2389 - 2392
反应条件
1: With trimethylsilyl trifluoromethanesulfonate; triphenylphosphine in dichloromethane
T=20°C; 1 h;
2: With diisobutylaluminium hydride in hexane; dichloromethane
T=-78°C; regioselective reaction;
参考文献
Yahata, Kenzo; Minami, Masaki; Yoshikawa, Yuki; Watanabe, Kei; Fujioka, Hiromichi
Chemical and Pharmaceutical Bulletin, 2013 , vol. 61, # 12 p. 1298 - 1307
反应条件
pyridine; air; Pd(II)-hydrotalcite in toluene
T=65°C; P=2280.15 Torr; 17 h;
参考文献
Kakiuchi; Maeda; Nishimura; Uemura
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6620 - 6625
