反应条件
1.1: hydroxylamine hydrochloride; sodium acetate / methanol; water / 20 °C
2.1: triethylamine; methanesulfonyl chloride / tetrahydrofuran / 0.5 h / 0 - 20 °C
2.2: 0.52 h
3.1: [Acr+-Mes]ClO4- / 1,2-dichloro-ethane / 16 h / 20 °C / |Schlenk technique; |Irradiation
4.1: water; lithium hydroxide hydrate / methanol; tetrahydrofuran / 40 h / |Reflux
View Scheme
参考文献
Xuan, Jun; Xia, Xu-Dong; Zeng, Ting-Ting; Feng, Zhu-Jia; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Angewandte Chemie - International Edition, 2014 , vol. 53, # 22 p. 5653 - 5656
Angew. Chem., 2014 , vol. 126, # 22 p. 5759 - 5762,4