1,1,3-三甲基环戊烷合成路线 (共 79 条)
反应条件
potassium hydroxide; hydrazine hydrate; diethylene glycol
参考文献
Gault; Germain
Bulletin de la Societe Chimique de France, 1959 , p. 1365,1367, 1370
反应条件
kieselguhr; nickel Hydrogenation;
参考文献
Auterinen
Suomen Kemistilehti B, 1954 , vol. 27, p. 29,32
反应条件
nickel Hydrogenation;
参考文献
Birch; Johnson
Journal of the Chemical Society, 1951 , p. 1493,1495
反应条件
nickel Hydrogenation;
参考文献
Birch; Johnson
Journal of the Chemical Society, 1951 , p. 1493,1495
反应条件
in tetrahydrofuran T=25°C; 0.5 h; also with NaPPh2 or KPPh2; other solvent; MechanismProduct distribution;
参考文献
Ashby, E. C.; Gurumurthy, R.; Ridlehuber, R. W.
Journal of Organic Chemistry, 1993 , vol. 58, # 21 p. 5832 - 5837
反应条件
magnesium in tetrahydrofuran T=25°C; 2 h; various reaction times and Mg excess investigated; Product distributionMechanism;
参考文献
Doctorovich, Fabio; Deshpande, Abhay K.; Ashby, E. C.
Tetrahedron, 1994 , vol. 50, # 20 p. 5945 - 5956
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=25°C; 30 h; also with LAD in THF-d8; other times; in the dark, lab light or irradiation; Product distributionMechanism;
参考文献
Ashby, E. C.; Deshpande, Abhay K.
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3798 - 3805
反应条件
1: aluminium oxide / 300 - 325 °C 2: Raney nickel / Hydrogenation View Scheme
参考文献
Birch; Johnson
Journal of the Chemical Society, 1951 , p. 1493,1495
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Dey; Linstead
Journal of the Chemical Society, 1935 , p. 1063
反应条件
hydrogen; titanium T=419.9°C; Rate constantProduct distributionThermodynamic data;
参考文献
Clarke, John K. A.; Hegarty, Bernard F.; Rooney, John J.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1988 , vol. 84, # 7 p. 2511 - 2518