反应条件
1: CuBr*Me2S / hexamethylphosphoric acid triamide; tetrahydrofuran / 3 h / -78 °C 2: H2O, H+ / 0.08 h 3: 1.) sodium hexamethyldisilazide / 1.) THF, reflux, 2 h, 2.) THF, a) -78 deg C, 2 h, b) RT, 12 h View Scheme
参考文献
Pikul, Stanislaw; Raczko, Jerzy; Jurczak, Janusz
Bulletin of the Polish Academy of Sciences, Chemistry, 1987 , vol. 35, # 7-8 p. 297 - 299
