4-甲基偶氮苯四氟硼酸盐合成路线 （共 216 条）
反应条件
trimethylsilylazide; 1-n-butyl-3-methylimidazolium hexafluorophosphate
T=65°C; 2 h;
参考文献
Hubbard, Abigail; Okazaki, Takao; Laali, Kenneth K.
Journal of Organic Chemistry, 2008 , vol. 73, # 1 p. 316 - 319
反应条件
sodium hydrogen selenide in ethanol; N,N-dimethyl-formamide
0.333333 h;
参考文献
Chen; Qiu; Zhou
Synthetic Communications, 1991 , vol. 21, # 17 p. 1729 - 1734
反应条件
(3aS,7aS)-1,3-di-o-tolyl-octahydro-benzoimidazole-2-thione; palladium diacetate in tetrahydrofuran
T=50°C; Suzuki reaction; 10 h;
参考文献
Mingji, Dai; Liang, Bo; Wang, Cuihua; You, Zejin; Xiang, Jing; Dong, Guangbin; Chen, Jiahua; Yang, Zhen
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1669 - 1673
反应条件
palladium diacetate in methanol
Heck reaction; 1 h; Heating;
参考文献
Sengupta; Sadhukhan; Singh
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 997 - 999
反应条件
potassium acetate; 18-crown-6 ether
1.5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Beadle, James R.; Korzeniowsky, Stephen H.; Rosenberg, David E.; Garcia-Slanga, Blanche J.; Gokel, George W.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1594 - 1603
反应条件
2,6-di-tert-butyl-4-methylpyridine; gold(I) chloride; palladium dichloride; SIDip*HCl in acetonitrile
T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
in ethanol
T=25°C; Heck Reaction; 24 h;
参考文献
Li, Xing; Wang, Li-Chao; Chang, Hong-Hong; Zhang, Cong-Xia; Wei, Wen-Long
Applied Catalysis A: General, 2013 , vol. 462-463, p. 15 - 22
反应条件
tetrabutyl-ammonium chloride; optical active ligand; copper trifluoromethanesulfonate in acetonitrile
T=0 - 5°C; enantioselectivity (some percent); var. olefinic substrates and diazonium salts; Br(1-) reagent also; acetone solvent also; var. ligands; at -40 deg C also; var. reagent and catalyst concentration; Product distribution;
参考文献
Brunner, Henri; Bluechel, Christian; Doyle, Michael P.
Journal of Organometallic Chemistry, 1997 , vol. 541, # 1-2 p. 89 - 95
反应条件
in methanol
T=20°C; 0.25 h; different amounts of educts; Product distribution;
参考文献
Yasui, Shinro; Shioji, Kosei; Ohno, Atsuyoshi
Tetrahedron Letters, 1994 , vol. 35, # 17 p. 2695 - 2698
反应条件
in methanol
T=20°C; 0.25 h;
参考文献
Yasui, Shinro; Shioji, Kosei; Ohno, Atsuyoshi
Tetrahedron Letters, 1994 , vol. 35, # 17 p. 2695 - 2698
