反应条件
1.1: sodium perborate tetrahydrate / 9 h / 40 °C 2.1: tert.-butyl lithium / diethyl ether; pentane / -78 - 0 °C / Inert atmosphere 2.2: 1 h / -78 - 20 °C / Inert atmosphere 3.1: tetramethyl-ammonium fluoride / acetonitrile / Inert atmosphere; Glove box 4.1: benzene-d6 / 0.25 h / 140 °C / Inert atmosphere; Glove box; Sealed tube View Scheme
参考文献
Graskemper, Joseph W.; Wang, Bijia; Qin, Linlin; Neumann, Kiel D.; Dimagno, Stephen G.
Organic Letters, 2011 , vol. 13, # 12 p. 3158 - 3161