4-甲氧苯重氮四氟硼酸盐合成路线 （共 231 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride in acetonitrile T=20°C; Stille reaction; 0.5 h;
参考文献
Hosoya, Takamitsu; Aoyama, Hiroshi; Ikemoto, Takaaki; Kihara, Yasutaka; Hiramatsu, Toshiyuki; Endo, Makoto; Suzuki, Masaaki
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 5 p. 663 - 673
反应条件
palladium diacetate in methanol T=20°C; Heck reaction; 24 h; Inert atmosphereDarkness; regioselective reaction;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio
Synlett, 2009 , # 8 p. 1277 - 1280
反应条件
palladium diacetate in methanol T=20°C; Heck reaction; 16 h; Inert atmosphereDarkness; regioselective reaction;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio
Synlett, 2009 , # 8 p. 1277 - 1280
反应条件
palladium diacetate in ethanol T=40°C; Heck reaction; 8 h; Inert atmosphereDarkness; regioselective reaction;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio
Synlett, 2009 , # 8 p. 1277 - 1280
反应条件
1: 86 percent / Pd(OAc)2 / 0.25 h / Ambient temperature 2: 88 percent / mCPBA, BF3*Et2O / CH2Cl2 / 0 deg C to r.t. 3: 71 percent / NBS, AIBN / CCl4 / Heating View Scheme
参考文献
Mehta, Goverdhan; Sengupta, Saumitra
Tetrahedron Letters, 1996 , vol. 37, # 47 p. 8625 - 8626
反应条件
sodium azide in methanol; hexane T=-40°C; 0.25 h;
参考文献
Schroer, Thorsten; Haiges, Ralf; Schneider, Stefan; Christe, Karl O.
Chemical Communications, 2005 , # 12 p. 1607 - 1609
反应条件
dibenzo-18-crown-6; potassium bromide; copper(ll) bromide; 1,10-phenanthroline; copper(I) bromide in acetonitrile T=20°C; Sandmeyer bromination; 0.333333 h;
参考文献
Synthesis, , # 16 p. 2534 - 2538
反应条件
sodium hydroxide in acetonitrile T=20°C;
参考文献
European Journal of Organic Chemistry, , # 22 p. 3837 - 3843
反应条件
trimethylsilyl bromide; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=55°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 1 p. 316 - 319
反应条件
iron(II) sulfate in water; dimethyl sulfoxide 0.166667 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9609 - 9616
