4-甲氧苯重氮四氟硼酸盐合成路线 （共 231 条）
反应条件
1: ethyl 3-bromobutane-1-carboxylate With chloro-trimethyl-silane; ethylene dibromide; lithium chloride; zinc in tetrahydrofuran T=25°C; 12 h; Inert atmosphere; 2: With zinc dibromide in tetrahydrofuran T=25°C; 0.166667 h; Inert atmosphere; 3: 4-methoxybenzenediazonium tetrafluoroborate With chloro-trimethyl-silane in tetrahydrofuran T=-60 - 125°C; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Zhang, Zhi-Guang; Haag, Benjamin A.; Li, Jin-Shan; Knochel, Paul
Synthesis, 2011 , # 1 p. 23 - 29
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine; sodium iodide in acetonitrile T=80°C; 24 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 20 p. 4518 - 4520
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine in acetonitrile T=80°C; 24 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 20 p. 4518 - 4520
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane T=100°C; P=760 Torr; 5 h;
参考文献
Tetrahedron Letters, , vol. 43, # 50 p. 9137 - 9140
反应条件
calcium carbonate; Lindlar's catalyst in methanol
参考文献
Brunner, Heiko; De Courcy, Nathalie Le Cousturier; Genet, Jean-Pierre
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4815 - 4818
反应条件
Further byproducts given;
参考文献
Todres, Z. V.; Ovsepyan, G. Ts.; Kosnikov, A. Yu.; Lindeman, S. V.; Struchkov, Yu. T.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2318 - 2321
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2567 - 2570
反应条件
Cu(BF4)2*6H2O in hexadeuterioacetone; water T=-10°C; Meerwein Arylation; 2.5 h;
参考文献
Baranovskii; Petrushka; Fesak; Grishchuk
Russian Journal of General Chemistry, 2013 , vol. 83, # 2 p. 325 - 328
Zh. Obshch. Khim., 2013 , vol. 83, # 2 p. 271 - 274,4
反应条件
iron(II) bis(thiocyanate) in water; acetone T=-40 - -20°C;
参考文献
Grishchuk, B. D.; Gorbovoi, P. M.; Ganushchak, N. I.; Brush, D. M.; Kudrik, E. Ya.
Russian Journal of General Chemistry, 1993 , vol. 63, # 7.2 p. 1156 - 1158
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 7 p. 1655 - 1658
反应条件
copper diacetate in water; acetone T=-40 - -30°C;
参考文献
Gorbovoi; Zagrichuk; Grichshuk
Russian Journal of General Chemistry, 2000 , vol. 70, # 5 p. 755 - 757
反应条件
1,1,2-trichloroethylene; Cu(SCN)2 in water; acetone T=-25 - -20°C; 1.5 h;
参考文献
Grishchuk, B. D.; Kudrik, E. Ya.; Gorbovoi, P. M.; Garmider, V. L.; Ganushchak, N. I.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.1 p. 1164 - 1166
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1294 - 1297
