4-甲氧苯重氮四氟硼酸盐合成路线 （共 231 条）
反应条件
magnesium 1.) THF, reflux, 2.) THF, 30 deg C, 180 s; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Singh, P. R.; Khanna, R. K.; Jayaraman, B.
Tetrahedron Letters, 1982 , vol. 23, # 51 p. 5475 - 5478
反应条件
1: With [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate in acetonitrile T=30°C; Heck reaction; 0.5 h; 2: With hydrogenchloride in water; acetonitrile T=25°C; 0.5 h;
参考文献
Machado, Angelo H.L.; de Sousa, Marcio A.; Patto, Daniela C.S.; Azevedo, Luiz F.S.; Bombonato, Fernanda I.; Correia, Carlos Roque D.
Tetrahedron Letters, 2009 , vol. 50, # 11 p. 1222 - 1225
反应条件
palladium diacetate in acetonitrile 0.5 h; Ambient temperature;
参考文献
Kikukawa, Kiyoshi; Idemoto, Tohru; Katayama, Atsuhiko; Kono, Kiyoshi; Wada, Fumio; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1511 - 1514
反应条件
in dimethyl sulfoxide 3 h; Ambient temperatureIrradiation;
参考文献
Citterio, Attilio; Serravalle, Marco; Vismara, Elena
Tetrahedron Letters, 1982 , vol. 23, # 17 p. 1831 - 1834
反应条件
copper in dimethyl sulfoxide T=20°C; 24 h; different biacetyl/benzene ratio; Rate constantMechanismProduct distribution;
参考文献
Citterio, Attilio; Vismara, Elena; Bernardi, Rosanna
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 876 - 890
反应条件
water; sodium acetate in acetonitrile
T=0°C; 1.16667 h; Inert atmosphere;
参考文献
Xia, Zhonghua; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 16 p. 4110 - 4113
反应条件
18-crown-6 ether; potassium acetate
参考文献
Ellames, George J; Gibson, Jennifer S; Herbert, John M; McNeill, Alan H
Tetrahedron, 2001 , vol. 57, # 46 p. 9487 - 9497
参考文献
MacHado, Angelo H. L.; Milagre, Humberto M. S.; Eberlin, Livia S.; Sabino, Adao A.; Correia, Carlos Roque D.; Eberlin, Marcos N.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 20 p. 3277 - 3281
反应条件
1: 1-bromocyclohexane With chloro-trimethyl-silane; magnesium; ethylene dibromide; lithium chloride; zinc dibromide in tetrahydrofuran
T=0 - 25°C; 4 h; Inert atmosphere;
2: With zinc dibromide in tetrahydrofuran
T=25°C; 0.166667 h; Inert atmosphere;
3: 4-methoxybenzenediazonium tetrafluoroborate With chloro-trimethyl-silane in tetrahydrofuran
T=-60 - 125°C; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Zhang, Zhi-Guang; Haag, Benjamin A.; Li, Jin-Shan; Knochel, Paul
Synthesis, 2011 , # 1 p. 23 - 29
反应条件
iron(II) sulfate in water; dimethyl sulfoxide
0.166667 h;
参考文献
Heinrich, Markus R.; Blank, Olga; Ullrich, Daniela; Kirschstein, Marcel
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9609 - 9616
