4-甲氧苯重氮四氟硼酸盐合成路线 (共 231 条)
反应条件
1: 4-methoxybenzenediazonium tetrafluoroborate With palladium diacetate in methanol
Suzuki-Miyaura reaction; 0.166667 h; Inert atmosphere;
2: potassium 3,4-(methylenedioxy)phenyltrifluoroborate in methanol
T=20°C; Suzuki-Miyaura reaction; 12 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Hoelter, Frank
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 13 p. 4914 - 4920
反应条件
in tetrahydrofuran
T=20°C; 4 h; Inert atmosphereGreen chemistry;
参考文献
Balaguez, Renata A.; Ricordi, Vanessa Gentil; Freitas, Camilo S.; Perin, Gelson; Schumacher, Ricardo F.; Alves, Diego
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1057 - 1061
反应条件
iron(II) sulfate in water; dimethyl sulfoxide
0.166667 h;
参考文献
Heinrich, Markus R.; Blank, Olga; Ullrich, Daniela; Kirschstein, Marcel
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9609 - 9616
反应条件
iron(II) sulfate in water; dimethyl sulfoxide
0.166667 h;
参考文献
Heinrich, Markus R.; Blank, Olga; Ullrich, Daniela; Kirschstein, Marcel
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9609 - 9616
反应条件
tris-(o-tolyl)phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethanol
T=40°C; Heck reaction; 2 h;
参考文献
Konno, Tsutomu; Yamada, Shigeyuki; Tani, Akinori; Miyabe, Tomotsugu; Ishihara, Takashi
Synlett, 2006 , # 18 p. 3025 - 3028
反应条件
tris-(o-tolyl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran
Heck reaction; 2 h; Heating; Product distribution; Further Variations:SolventsTemperatures;
参考文献
Konno, Tsutomu; Yamada, Shigeyuki; Tani, Akinori; Miyabe, Tomotsugu; Ishihara, Takashi
Synlett, 2006 , # 18 p. 3025 - 3028
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane
T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
(IMes)Pd(NQ) in ethanol
T=50°C; Suzuki Coupling; 1 h; Conversion of starting material;
参考文献
Karch, Ralf; Briel, Oliver; Kayser, Bernd; Beller, Matthias; Selvakumar, Kumaravel; Frisch, Anja; Zapf, Alexander
Patent: US2006/122398 A1, 2006 ;
Location in patent: Page/Page column 8-9 ;
反应条件
alginate/gellan gum beads containing Pd nanoparticles in water
T=40°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Cacchi, Sandro; Caponetti, Eugenio; Casadei, Maria Antonietta; Di Giulio, Andrea; Fabrizi, Giancarlo; Forte, Giovanni; Goggiamani, Antonella; Moreno, Sandra; Paolicelli, Patrizia; Petrucci, Francesco; Prastaro, Alessandro; Saladino, Maria Luisa
Green Chemistry, 2012 , vol. 14, # 2 p. 317 - 320
反应条件
sodium hydrogen telluride in N,N-dimethyl-formamide
0.25 h;
参考文献
Chen; Qiu; Zhou
Synthetic Communications, 1991 , vol. 21, # 17 p. 1729 - 1734