3-(4-甲基苯甲酰)丙酸合成路线 （共 57 条）
反应条件
perchloric acid; NCSacc in water; acetic acid T=29.84°C; 24 h; Kinetics; Further Variations:Temperaturesvarious concentrations of substrate, reagents and rations of solvents;
参考文献
Limpricht; Doll
Justus Liebigs Annalen der Chemie, 1900 , vol. 312, p. 111
反应条件
sodium hydroxide; sodium hydrogencarbonate; sodium carbonate; potassium hexacyanoferrate(III); osmium(VIII) oxide in water T=36.85°C; pH=10.33; Kinetics; Further Variations:pH-values;
参考文献
Reddy, Cherkupally Sanjeeva; Manjari, Padma Sunitha
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2010 , vol. 49, # 4 p. 418 - 424
反应条件
potassium permanganate; perchloric acid; sodium perchlorate; NAF; acetic acid in water T=29.9°C; var. temperatures; ΔH(excit.), ΔS(excit.); Rate constantKineticsThermodynamic data;
参考文献
Sikkandar, G.; Ahamed, K. A. Basheer; Kannan, S.
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1992 , vol. 31, # 11 p. 845 - 848
反应条件
acetic acid in water T=30°C; KineticsMechanism; ConcentrationTemperature;
参考文献
Mohamed Farook; Alhaji; Uduman Mohideen; Seyed Dameen; Mitu, Liviu; Abshana Begam
Journal of Solution Chemistry, 2013 , vol. 42, # 6 p. 1183 - 1193
反应条件
disodium hydrogenphosphate; sodium acetate; permanganate(VII) ion T=29.85°C; Oxidation; pH=6.5; Kinetics; Further Variations:TemperaturesReagents;
参考文献
Sikkandar; Ahamed, K.A.Basheer; Kannan
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 1999 , vol. 38, # 2 p. 183 - 186
参考文献
Limpricht; Doll
Justus Liebigs Annalen der Chemie, 1900 , vol. 312, p. 111
反应条件
pyridine; lead(IV) acetate; copper diacetate
参考文献
Sane,P.P. et al.
Synthesis, 1973 , p. 541 - 542
反应条件
1: (i) N2H4, KOH, HOCH2CH2OH, (ii) polyphosphoric acid
View Scheme
参考文献
Baker; Hopkins
Journal of medicinal chemistry, 1970 , vol. 13, # 1 p. 87 - 89
反应条件
1: 72 percent / zinc amalgam, aq. HCl / toluene; H2O / 20 h / Heating
2: 83 percent / polyphosphoric acid / 0.12 h / 90 °C
3: 77 percent / zinc amalgam, aq. HCl / toluene; H2O / 20 h / Heating
View Scheme
参考文献
Collins, Michael J.; Gready, Jill E.; Sternhell, Sever; Tansey, Charles W.
Australian Journal of Chemistry, 1990 , vol. 43, p. 1547 - 1557
反应条件
1: H2SO4 / Heating
2: 100 percent / bromine / AlCl3 / diethyl ether; CCl4 / 0.08 h
3: 31 percent / NaBH4, NaHCO3 / methanol; H2O / 1.5 h / 28 °C
4: 95 percent / BF3*OEt2 / benzene / 1.5 h / Ambient temperature
View Scheme
参考文献
Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 5 p. 355 - 358
