1: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min 2: 93 percent / 30percent aq. KOH / methanol / 1 h / Ambient temperature 3: 89 percent / sodium benzeneselenolate / ethanol / 0.08 h / Ambient temperature View Scheme
参考文献
Satoh, Tsuyoshi; Kaneko, Youhei; Izawa, Takao; Sakata, Kiichi; Yamakawa, Koji
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 1983 - 1990
1: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min 2: 93 percent / 30percent aq. KOH / methanol / 1 h / Ambient temperature 3: 89 percent / sodium benzeneselenolate / ethanol / 0.08 h / Ambient temperature View Scheme
参考文献
Satoh, Tsuyoshi; Kaneko, Youhei; Izawa, Takao; Sakata, Kiichi; Yamakawa, Koji
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 1983 - 1990
1: 93 percent / 30percent aq. KOH / methanol / 1 h / Ambient temperature 2: 89 percent / sodium benzeneselenolate / ethanol / 0.08 h / Ambient temperature View Scheme
参考文献
Satoh, Tsuyoshi; Kaneko, Youhei; Izawa, Takao; Sakata, Kiichi; Yamakawa, Koji
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 1983 - 1990
in acetonitrile Ambient temperatureelectrochemical synthesis: divided cell, Pt plate electrodes, -2.30 V vs Ag/Ag(+), <Bu4N>I as supporting electrolyte;
参考文献
Yoshida, Kunihisa; Kuwata, Hideki
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 15 p. 1873 - 1877
