3,3-二甲基-2-丁醇合成路线 (共 125 条)
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; Pd((-)-sparteine)2Cl2 in tert-butyl alcohol T=65°C; 20 h;
参考文献
Mandal, Sunil K.; Jensen, David R.; Pugsley, Jacob S.; Sigman, Matthew S.
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4600 - 4603
反应条件
[(C4Ph4COHOCC4Ph4)(μ-H)][(CO)4Ru2]; Novozym(R) 435; 2,4-dimethylpentan-3-one in toluene T=70°C; P=157.513 Torr; 40 h;
参考文献
Verzijl, Gerard K.M.; De Vries, Johannes G.; Broxterman, Quirinus B.
Tetrahedron Asymmetry, 2005 , vol. 16, # 9 p. 1603 - 1610
反应条件
Sodium bromate; sulfuric acid; sodium bromide in water T=33 - 35°C; 0.75 h; Microwave irradiation;
参考文献
Paeaekkoenen, Sanna; Pursiainen, Jouni; Lajunen, Marja
Tetrahedron Letters, 2010 , vol. 51, # 51 p. 6695 - 6699
反应条件
palladium diacetate; oxygen; (-)-sparteine in 1,2-dichloro-ethane T=80°C; Title compound not separated from byproducts.;
参考文献
Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 14 p. 2730 - 2732
反应条件
[bis(acetoxy)iodo]benzene; potassium bromide in dichloromethane; water T=20°C; 1 h;
参考文献
Sun, Wei; Wu, Xiaomei; Xia, Chungu
Helvetica Chimica Acta, 2007 , vol. 90, # 3 p. 623 - 626
反应条件
chromium(VI) oxide; acetic acid
参考文献
Mosher; Whitmore
Journal of the American Chemical Society, 1948 , vol. 70, p. 2545
反应条件
[bis(acetoxy)iodo]benzene; potassium bromide; (S,S)-(+)-Jacobsen salene complex in dichloromethane T=20°C; 1 h; Kinetics; Further Variations:Solvents;
参考文献
Li, Zhen; Tang, Zhong H.; Hu, Xiao X.; Xia, Chun G.
Chemistry - A European Journal, 2005 , vol. 11, # 4 p. 1210 - 1216
参考文献
Mosher; Whitmore
Journal of the American Chemical Society, 1948 , vol. 70, p. 2545
反应条件
in acetonitrile T=60°C; Kinetics;
参考文献
Lu, Yun; Bradshaw, Joshua; Zhao, Yu; Kuester, William; Kabotso, Daniel
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 12 p. 1172 - 1178
参考文献
Toivonen
Annales Academiae Scientiarum Fennicae, Series A2: Chemica, 1956 , # 72 p. 27,32
Suomen Kemistilehti B, 1952 , vol. 25, p. 69,72