3Α-羟基-7-氧代-5Β-胆烷酸合成路线 （共 33 条）
参考文献
Iwasaki
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1936 , vol. 244, p. 181,188
参考文献
Iwasaki
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1936 , vol. 244, p. 181,188
反应条件
1: HCl 2: pyridine 3: bromine; HBr; acetic acid 4: aqueous methanol. KOH / 20 °C 5: NaBH4; methanol View Scheme
参考文献
Hsia et al.
Journal of Biological Chemistry, 1957 , vol. 225, p. 811,818
Journal of Biological Chemistry, 1958 , vol. 233, p. 1337
反应条件
sodium tetrahydroborate; sodium hydrogencarbonate in water T=20°C; 0.5 h; var. reducing agents;
参考文献
Giovannini, Pier Paolo; Grandini, Alessandro; Perrone, Daniela; Pedrini, Paola; Fantin, Giancarlo; Fogagnolo, Marco
Steroids, 2008 , vol. 73, # 14 p. 1385 - 1390
参考文献
Miyazi
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1937 , vol. 250, p. 31
参考文献
Iwasaki
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1936 , vol. 244, p. 181,188
参考文献
Miyazi
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1937 , vol. 250, p. 31
反应条件
1: HCl 2: pyridine 3: bromine; HBr; acetic acid 4: aqueous methanol. KOH / 20 °C 5: boron fluoride ether adduct 6: Raney nickel; aqueous ethanol View Scheme
参考文献
Hsia et al.
Journal of Biological Chemistry, 1957 , vol. 225, p. 811,818
Journal of Biological Chemistry, 1958 , vol. 233, p. 1337
反应条件
1: sodium; propan-1-ol 2: H2SO4 View Scheme
参考文献
Proceedings of the Japan Academy, , vol. 30, p. 391
反应条件
hydrogenchloride; acetic acid; platinum Hydrogenation;
参考文献
Bovara, Roberto; Canzi, Enrica; Carrea, Giacomo; Pilotti, Alessandra; Riva, Sergio
Journal of Organic Chemistry, 1993 , vol. 58, # 2 p. 499 - 501
