2,4,4-三甲基环戊酮合成路线 （共 37 条）
反应条件
nickel in tetrahydrofuran; water T=20°C; 1.5 h;
参考文献
Tetrahedron, , vol. 63, # 16 p. 3367 - 3379
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 5008 - 5009
反应条件
sulfuric acid in 1,4-dioxane 1) 20 deg C, 18 h, 2) 80-84 deg C, 3 h;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 94, # 1 p. 75 - 80
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Journal of the Chemical Society, , p. 1063
反应条件
bis(benzonitrile)palladium(II) dichloride; hydrogen 1.) benzene, 8-10 deg C, 2 h; acetonitrile, reflux, 2 h, 2.) benzene, 1 atm, 1 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 4519
反应条件
barium dihydroxide; manganese dihydrogen carbonate T=250 - 255°C;
参考文献
Journal of Organic Chemistry, , vol. 25, p. 514 - 518
反应条件
1.1: 30percent H2O2; NaOH (6M) / methanol / 15 - 20 °C 1.2: 65 percent / Na2SO3; NaHCO3 / H2O; methanol 2.1: 76 percent Spectr. / BF3*Et2O / benzene / 0.17 h / 20 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 10 p. 1905 - 1911
反应条件
1: aluminum amalgam / diethyl ether 2: mercuric chloride, H2O / acetonitrile View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 5008 - 5009
反应条件
1: (i) aq. H2O2, HCO2H, (ii) aq. NaMnO4 2: Ba(OH)2, MnCO3 / 250 - 255 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 25, p. 514 - 518
反应条件
1: (i) H2, Ni, (ii) TsOH 2: (i) aq. H2O2, HCO2H, (ii) aq. NaMnO4 3: Ba(OH)2, MnCO3 / 250 - 255 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 25, p. 514 - 518
