1-((4-甲基苯基)磺酰)哌啶合成路线 (共 60 条)
反应条件
di-tert-butyl peroxide in chlorobenzene
Heating;
参考文献
Ouvry, Gilles; Quiclet-Sire, Beatrice; Zard, Samir Z.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 30 p. 5002 - 5006
反应条件
sodium tetrahydroborate; iron(II) chloride in acetonitrile
T=50°C; 16 h; Inert atmosphere;
参考文献
Ekomie, Audrey; Lefevre, Guillaume; Fensterbank, Louis; Lacote, Emmanuel; Malacria, Max; Ollivier, Cyril; Jutand, Anny
Angewandte Chemie - International Edition, 2012 , vol. 51, # 28 p. 6942 - 6946
反应条件
1: With 2,4,6-trichloro-1,3,5-triazine in acetonitrile
T=20°C; 0.5 h;
2: With triethylamine in acetonitrile
参考文献
Rad, Mohammad Navid Soltani; Khalafi-Nezhad, Ali; Asrari, Zeinab; Behrouz, Somayeh; Amini, Zohreh; Behrouz, Marzieh
Synthesis, 2009 , # 23 art. no. Z15009SS, p. 3983 - 3988
反应条件
[Ir(μ-Cl)(cyclooctene)2]2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; lithium chloride in water; 1,3,5-trimethyl-benzene
T=170°C; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Olsen, Esben P. K.; Madsen, Robert
Chemistry - A European Journal, 2012 , vol. 18, # 50 p. 16023 - 16029
反应条件
[BMIM][AlCl4]
T=20°C; 0.5 h;
参考文献
Naik, Prashant U.; Harjani, Jitendra R.; Nara, Susheel J.; Salunkhe, Manikrao M.
Tetrahedron Letters, 2004 , vol. 45, # 9 p. 1933 - 1936
反应条件
1: toluene-4-sulfonamide With sodium hydride in N,N-dimethyl-formamide
T=20°C; 0.5 h;
2: 5-bromopentyldiphenylsulfonium trifluoromethanesulfonate in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Yamanaka, Hiroyuki; Yamane, Yoshinobu; Mukaiyama, Teruaki
Heterocycles, 2004 , vol. 63, # 12 p. 2813 - 2826
反应条件
[Ni0(1,5-cyclooctadiene)2]; zinc; (4-Cl)-H-PyBox in N,N-dimethyl acetamide
T=25°C; 16 h; Inert atmosphere;
参考文献
Yu, Xiaolong; Yang, Tao; Wang, Shulin; Xu, Hailiang; Gong, Hegui
Organic Letters, 2011 , vol. 13, # 8 p. 2138 - 2141
反应条件
sodium hypochlorite in water
Ambient temperature;
参考文献
Scully, Frank E.; Bowdring, Katherine
Journal of Organic Chemistry, 1981 , vol. 46, p. 5077 - 5081
反应条件
in tetrahydrofuran
T=20°C; 20 h;
参考文献
Katritzky, Alan R.; Rodriguez-Garcia, Valerie; Nair, Satheesh K.
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 1849 - 1852
反应条件
1: toluene-4-sulfonamide With sodium hydride in N,N-dimethyl-formamide
T=20°C; 0.5 h;
2: 1,5-dibromo-pentane in N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Yamanaka, Hiroyuki; Yamane, Yoshinobu; Mukaiyama, Teruaki
Heterocycles, 2004 , vol. 63, # 12 p. 2813 - 2826