1: diethyl ether; aqueous NaOH-solution; chloroform 2: phosphoryl chloride; toluene View Scheme

hydrogen; nickel in ethanol P=2844.3 Torr;

1: 44 percent / methanol 2: 78 percent / H2 / Raney Ni / ethanol / 2844.3 Torr View Scheme

1: 89 percent / ammonium acetate / benzene / 6 h / Heating 2: 44 percent / methanol 3: 78 percent / H2 / Raney Ni / ethanol / 2844.3 Torr View Scheme

ethanol; ammonia T=110°C;

暂无反应条件数据

1: 91.2 percent / 10percent aq. NaOH / diethyl ether / 1 h / 0 - 5 °C 2: 64.7 percent / POCl3 / toluene / 2.5 h / 120 °C 3: 82.4 percent / dimethylformamide / 5 h / 180 °C 4: 40.7 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating 5: 69.5 percent / polyphosphoric acid / 1 h / 100 °C 6: 41.5 percent / Ag2O / methanol; CHCl3 / 6 h / 60 °C View Scheme

1: 91.2 percent / 10percent aq. NaOH / diethyl ether / 1 h / 0 - 5 °C 2: 64.7 percent / POCl3 / toluene / 2.5 h / 120 °C 3: 82.4 percent / dimethylformamide / 5 h / 180 °C 4: 40.7 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating View Scheme

1: 81.9 percent / 10percent aq. NaOH / diethyl ether / 1 h / 0 - 5 °C 2: 54.2 percent / POCl3 / toluene / 2.5 h / 120 °C 3: 70.9 percent / dimethylformamide / 5 h / 180 °C 4: 41.1 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating 5: 64.1 percent / polyphosphoric acid / 1 h / 100 °C View Scheme

1: 81.9 percent / 10percent aq. NaOH / diethyl ether / 1 h / 0 - 5 °C 2: 54.2 percent / POCl3 / toluene / 2.5 h / 120 °C 3: 70.9 percent / dimethylformamide / 5 h / 180 °C 4: 41.1 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating 5: 64.1 percent / polyphosphoric acid / 1 h / 100 °C 6: 67 percent / Ag2O / methanol; CHCl3 / 6 h / 60 °C View Scheme