联苯-4,4-草酸二乙酯合成路线 （共 84 条）
反应条件
manganese; cobalt (II) bromide; triphenylphosphine; trifluoroacetic acid in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Amatore, Muriel; Gosmini, Corinne
Angewandte Chemie - International Edition, 2008 , vol. 47, # 11 p. 2089 - 2092
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,1'-bis(diphenylphosphino)ferrocene; Ph–ZnI in tetrahydrofuran T=40°C; Negishi coupling reaction; 1 h; Inert atmosphere;
参考文献
Takahashi, Hideki; Inagaki, Shinya; Yoshii, Naoko; Gao, Fuxing; Nishihara, Yasushi; Takagi, Kentaro
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2794 - 2797
反应条件
1: With [resin-CH2N(CH3)3]2CO3; Pd(PAnPh2)2Cl2 in water; N,N-dimethyl-formamide T=80°C; Suzuki coupling; 16 h; 2: With maleimido-CH2-PS resin in water; N,N-dimethyl-formamide T=90°C; 10 h;
参考文献
Lan, Ping; Berta, Daniela; Porco Jr., John A.; South, Michael S.; Parlow, John J.
Journal of Organic Chemistry, 2003 , vol. 68, # 25 p. 9678 - 9686
反应条件
manganese; water; trifluoroacetic acid; Co(2,2'-bipyridine)Br2; lithium bromide in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Amatore, Muriel; Gosmini, Corinne; Perichon, Jacques
Journal of Organic Chemistry, 2006 , vol. 71, # 16 p. 6130 - 6134
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=120°C;
参考文献
Zhang, Daohua; Liu, Zhijian; Yum, Eul K.; Larock, Richard C.
Journal of Organic Chemistry, 2007 , vol. 72, # 1 p. 251 - 262
反应条件
lithium tetrachloromanganate(II); air in tetrahydrofuran T=-20°C; 0.75 h;
参考文献
Kiefer, Gregor; Jeanbourquin, Loic; Severin, Kay
Angewandte Chemie - International Edition, 2013 , vol. 52, # 24 p. 6302 - 6305
Angew. Chem., 2013 , vol. 125, # 24 p. 6422 - 6425
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); potassium iodide; zinc in tetrahydrofuran; N,N-dimethyl-formamide T=67°C; 4 h;
参考文献
Jutand, Anny; Mosleh, Adil
Journal of Organic Chemistry, 1997 , vol. 62, # 2 p. 261 - 274
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc dibromide in acetonitrile the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis;
参考文献
Fillon, Hyacinthe; Gosmini, Corinne; Perichon, Jacques
Journal of the American Chemical Society, 2003 , vol. 125, # 13 p. 3867 - 3870
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc dibromide in acetonitrile the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis;
参考文献
Fillon, Hyacinthe; Gosmini, Corinne; Perichon, Jacques
Journal of the American Chemical Society, 2003 , vol. 125, # 13 p. 3867 - 3870
反应条件
1: With [resin-CH2N(CH3)3]2CO3 in water; N,N-dimethyl-formamide T=80°C; Suzuki coupling; 16 h; 2: With [resin-CH2N(CH3)3]2CO3; 4-{[(9-anthrylmethyl)amino]carbonyl}phenylboronic acid in water; N,N-dimethyl-formamide T=80°C; 3: With maleimido-CH2-PS resin in water; N,N-dimethyl-formamide T=90°C; 10 h;
参考文献
Lan, Ping; Berta, Daniela; Porco Jr., John A.; South, Michael S.; Parlow, John J.
Journal of Organic Chemistry, 2003 , vol. 68, # 25 p. 9678 - 9686
