联苯-4,4-草酸二乙酯合成路线 （共 84 条）
反应条件
1: benzoyl chloride With indium; chloro-trimethyl-silane; ethylene dibromide; lithium chloride in tetrahydrofuran; dimethyl sulfoxide T=40°C; 3 h; Inert atmosphere; 2: 4-iodobenzoic acid ethyl ester With tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran; dimethyl sulfoxide T=25°C; 12 h; Inert atmosphere; Reagent/catalystSolventTemperatureTime;
参考文献
Lee, Dohyung; Ryu, Taekyu; Park, Youngchul; Lee, Phil Ho
Organic Letters, 2014 , vol. 16, # 4 p. 1144 - 1147
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
samarium; triphenylphosphine; nickel dichloride in N,N-dimethyl-formamide T=70°C; 8 h;
参考文献
Zheng, Xingliang; Zhang, Yongmin
Journal of Chemical Research - Part S, 2002 , # 11 p. 562 - 563
反应条件
water; caesium carbonate; 1,4-di(diphenylphosphino)-butane; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=90°C; 24 h; Title compound not separated from byproducts;
参考文献
Denmark, Scott E.; Ober, Michael H.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1703 - 1714
反应条件
water; caesium carbonate; 1,4-di(diphenylphosphino)-butane; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=110°C; 24 h;
参考文献
Denmark, Scott E.; Ober, Michael H.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1703 - 1714
反应条件
water; caesium carbonate; 1,4-di(diphenylphosphino)-butane; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=90°C; 18 h; Title compound not separated from byproducts;
参考文献
Denmark, Scott E.; Ober, Michael H.
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1703 - 1714
反应条件
1: benzoyl chloride With indium; chloro-trimethyl-silane; ethylene dibromide; lithium chloride in N,N-dimethyl-formamide T=40°C; 3 h; Inert atmosphere; 2: 4-iodobenzoic acid ethyl ester With tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide T=90°C; 5 h; Inert atmosphere;
参考文献
Lee, Dohyung; Ryu, Taekyu; Park, Youngchul; Lee, Phil Ho
Organic Letters, 2014 , vol. 16, # 4 p. 1144 - 1147
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
