2-苯基-4-五亚乙基六胺-2-醇合成路线 (共 59 条)
反应条件
lithium in tetrahydrofuran 0.05 h; ultrasonication;
参考文献
Araki, Shuki; Butsugan, Yasuo
Chemistry Letters, 1988 , p. 457 - 458
反应条件
hydrogenchloride; water in methanol T=20°C;
参考文献
Ito, Suguru; Hayashi, Akira; Komai, Hirotomo; Yamaguchi, Hitoshi; Kubota, Yoshihiro; Asami, Masatoshi
Tetrahedron, 2011 , vol. 67, # 11 p. 2081 - 2089
反应条件
bis(benzonitrile)palladium(II) dichloride; tin(ll) chloride in various solvent(s) T=50°C; 45 h;
参考文献
Takahara, Jun P.; Masuyama, Yoshiro; Kurusu, Yasuhiko
Journal of the American Chemical Society, 1992 , vol. 114, # 7 p. 2577 - 2586
反应条件
(S)-BIPHEN in toluene T=0°C; 15 h;
参考文献
Lou, Sha; Moquist, Philip N.; Schaus, Scott E.
Journal of the American Chemical Society, 2006 , vol. 128, # 39 p. 12660 - 12661
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 6 h;
参考文献
Reilly, Maureen K.; Rychnovsky, Scott D.
Organic Letters, 2010 , vol. 12, # 21 p. 4892 - 4895
反应条件
2,6-dimethylpyridine; zinc trifluoromethanesulfonate in dichloromethane T=20°C; 24 h; Product distribution; Further Variations:CatalystsReaction partnersReagentsSolventscatalyst and reagent ratios, reaction time;
参考文献
Hamasaki; Chounan; Horino; Yamamoto
Tetrahedron Letters, 2000 , vol. 41, # 50 p. 9883 - 9887
反应条件
1: 2-phenyl-2-methyl-1,3-dioxolane With sodium lauryl sulfate; toluene-4-sulfonic acid in hexane; water 4.25 h; 2: vinyl-magnesium bromide in tetrahydrofuran; diethyl ether; hexane 16 h; Further stages.;
参考文献
Runge, M. Brett; Mwangi, Martin T.; Miller II, A. Lee; Perring, Mathew; Bowden, Ned B.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 5 p. 935 - 939
反应条件
In(OSO2CF3)3 in dichloromethane T=20°C; 12 h;
参考文献
Liu, Ling-Yan; Tang, Long; Yu, Lei; Chang, Wei-Xing; Li, Jing
Tetrahedron, 2005 , vol. 61, # 46 p. 10930 - 10934
反应条件
toluene-4-sulfonic acid in toluene T=40°C; 24 h;
参考文献
Matsuoka, Hiroaki; Kondo, Kazuhiro
Tetrahedron Letters, 2009 , vol. 50, # 20 p. 2320 - 2321
反应条件
tetrabutylammomium bromide; cadmium in tetrahydrofuran 8 h; Ambient temperatureother ketones, aldehydes, imines; other allyl halogenides;
参考文献
Sain, Bir; Prajapati, Dipak; Sandhu, Jagir S.
Tetrahedron Letters, 1992 , vol. 33, # 33 p. 4795 - 4798