反应条件
1: sodium azide / N,N,N',N',N'',N''-hexamethylphosphoric triamide / 0 - 20 °C / Inert atmosphere
2: potassium hydroxide / ethanol / 1 h / Inert atmosphere; Cooling with ice
3: pyridine; acetic anhydride / 20 °C / Inert atmosphere
4: 5,10,15,20-tetraphenyl-21H,23H-porphine Co(II) / toluene / 16 h / 75 °C / Inert atmosphere; Molecular sieve; Sealed tube
View Scheme
参考文献
Stokes, Benjamin J.; Liu, Sheng; Driver, Tom G.
Journal of the American Chemical Society, 2011 , vol. 133, # 13 p. 4702 - 4705