N-(3-硝基苯基)苯甲酰胺合成路线 （共 21 条）
反应条件
1: HCl, Fe, H2 / H2O; ethanol / 0.5 h / Heating 2: 89 percent / NaHCO3, NaOH / H2O / 8 h / 15 - 25 °C View Scheme
参考文献
Thiel, W.; Mayer, R.; Jauer, E.-A.; Modrow, H.; Dost, H.
Journal fuer Praktische Chemie (Leipzig), 1986 , vol. 328, # 4 p. 497 - 514
反应条件
lithium aluminium tetrahydride in diethyl ether 3 h; Heating;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 43, # 2 p. 432 - 436
反应条件
1: palladium 10 on activated carbon; ammonium formate / isopropyl alcohol / Inert atmosphere; Microwave irradiation 2: acetone / 1 h / Inert atmosphere; Reflux View Scheme
参考文献
Solinas, Antonio; Faure, Helene; Roudaut, Hermine; Traiffort, Elisabeth; Schoenfelder, Angele; Mann, Andre; Manetti, Fabrizio; Taddei, Maurizio; Ruat, Martial
Journal of Medicinal Chemistry, 2012 , vol. 55, # 4 p. 1559 - 1571
反应条件
lithium aluminium tetrahydride in diethyl ether 3 h; Heating;
参考文献
Joseph; Jacob, Dominic E.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 2 p. 432 - 436
反应条件
palladium 10 on activated carbon; hydrogen P=1034.32 Torr; 6 h;
参考文献
Barrett, Oscene V.; Downer-Riley, Nadale K.; Jackson, Yvette A.
Synthesis (Germany), 2012 , vol. 44, # 16 p. 2579 - 2586
反应条件
magnesium oxide in neat (no solvent)
T=70°C; 0.316667 h; Green chemistry; chemoselective reaction;
参考文献
Das, Vijay Kumar; Devi, Rashmi Rekha; Thakur, Ashim Jyoti
Applied Catalysis A: General, 2013 , vol. 456, p. 118 - 125
反应条件
copper(I) oxide; water; caesium carbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate; sodium hydroxide; N-methyl-2-(methylamino)ethylamine
T=100°C; 12 h; Inert atmosphereSealed tube;
参考文献
Wang, Jichao; Yin, Xinchi; Wu, Jun; Wu, Datong; Pan, Yuanjiang
Tetrahedron, 2013 , vol. 69, # 48 p. 10463 - 10469
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in acetone
T=20°C;
参考文献
Al-Nadaf, Afaf; Sheikha, Ghassan Abu; Taha, Mutasem O.
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 9 p. 3088 - 3115
反应条件
zinc in N,N-dimethyl-formamide
0.0333333 h; microwave irradiation;
参考文献
Arora, Revika; Paul, Satya; Gupta, Rajive
Canadian Journal of Chemistry, 2005 , vol. 83, # 8 p. 1137 - 1140
反应条件
2,6-dimethylpyridine in methanol; water
T=80°C; Microwave irradiation;
参考文献
Spiteri, Christian; Moses, John E.
Synlett, 2012 , vol. 23, # 10 art. no. ST-2012-D0154-L, p. 1546 - 1548
