1,2-二氢苯[J]并苊合成路线 （共 11 条）
反应条件
hydrogen iodide; hypophosphorous ether; acetic acid
0.025 h; Heating;
参考文献
Harvey, Ronald G.; Cortez, Cecilia
Journal of Organic Chemistry, 1987 , vol. 52, # 2 p. 283 - 284
反应条件
platinum
T=290 - 310°C; Erhitzen unter CO2;
参考文献
Cook; Haslewood
Journal of the Chemical Society, 1935 , p. 767,769
反应条件
hydrogenchloride; amalgamated zinc; acetic acid
weiteres Reagens: Toluol;
参考文献
Bachmann
Journal of Organic Chemistry, 1938 , vol. 3, p. 434,442
反应条件
T=400 - 410°C; unter Stickstoff;
参考文献
Bachmann
Journal of Organic Chemistry, 1938 , vol. 3, p. 434,442
Full Text Show Details
Fieser; Seligman
Journal of the American Chemical Society, 1935 , vol. 57, p. 2174
反应条件
1: Reduktion nach Clemmensen
2: platinum / 290 - 310 °C / Erhitzen unter CO2
View Scheme
参考文献
Cook; Haslewood
Journal of the Chemical Society, 1935 , p. 767,769
反应条件
(i) LiAlH4, (ii) Pd-C; Multistep reaction;
参考文献
Buchta,E.; Meyer,K.
Chemische Berichte, 1962 , vol. 95, p. 213 - 221
反应条件
(i) Zn-Hg, aq. HCl, EtOH, (ii) Pt-C, (dehydrogenation); Multistep reaction;
参考文献
Dannenberg,H.; Dannenberg- von Dresler,D.
Z. Naturforsch., B: Anorg. Chem., Org. Chem., Biochem., Biophys.,, 1964 , vol. 19, p. 801 - 806
反应条件
1: (i) PCl5, benzene, (ii) SnCl4
2: (i) Zn-Hg, aq. HCl, EtOH, (ii) Pt-C, (dehydrogenation)
View Scheme
参考文献
Dannenberg,H.; Dannenberg- von Dresler,D.
Z. Naturforsch., B: Anorg. Chem., Org. Chem., Biochem., Biophys.,, 1964 , vol. 19, p. 801 - 806
参考文献
Bachmann
Journal of Organic Chemistry, 1938 , vol. 3, p. 434,442
反应条件
diethyl ether; sodium; benzene
anschliessende Behandlung mit Methanol;
参考文献
Bachmann
Journal of Organic Chemistry, 1938 , vol. 3, p. 434,442
