4-甲基-1-戊烯-3-醇合成路线 （共 26 条）
反应条件
monoaluminum phosphate T=300 - 310°C;
参考文献
Nasarow; Mawrow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 472,482; engl. Ausg. S. 446, 454
参考文献
Nasarow; Mawrow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 472,482; engl. Ausg. S. 446, 454
反应条件
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide in dichloromethane 22 h;
参考文献
Rickerby, Jenny; Vallet, Martial; Bernardinelli, Gerald; Viton, Florian; Kuendig, E. Peter
Chemistry - A European Journal, 2007 , vol. 13, # 12 p. 3354 - 3368
反应条件
in tetrahydrofuran
T=0°C;
参考文献
Greeves, Nicholas; Lee, Wai-Man; Barkley, Jim V.
Tetrahedron Letters, 1997 , vol. 38, # 36 p. 6453 - 6456
反应条件
quinoline; hydrogen; Lindlar catalyst in pentane
P=760 Torr;
参考文献
Less, Simon L.; Handa, Sandeep; Millburn, Karen; Leadlay, Peter F.; Dutton, Christopher J.; Staunton, James
Tetrahedron Letters, 1996 , vol. 37, # 20 p. 3515 - 3518
反应条件
potassium tert-butylate in tetrahydrofuran
T=-78 - 0°C; Ramberg-Baecklund reaction;
参考文献
Makosza, Mieczyslaw; Urbanska, Natalia; Chesnokov, Alexey A.
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1473 - 1475
反应条件
1: With tert.-butyl lithium in tetrahydrofuran; hexane
T=-78 - 20°C; 3.5 h;
2: With dihydrogen peroxide; sodium hydroxide in tetrahydrofuran; hexane; water
T=0 - 20°C;
参考文献
Smith, Keith; Elliott, Mark C.; Jones, D. Heulyn
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9526 - 9531
反应条件
NH4PF6; cyclopentadienyl(1,5-cyclooctadiene)ruthenium chloride
T=100°C; 2 h;
参考文献
Trost, Barry M.; Martinez, Jose A.; Kulawiec, Robert J.; Indolese, Adriano F.
Journal of the American Chemical Society, 1993 , vol. 115, # 22 p. 10402 - 10403
反应条件
in diethyl ether
T=0°C; 3 h;
参考文献
Rickerby, Jenny; Vallet, Martial; Bernardinelli, Gerald; Viton, Florian; Kuendig, E. Peter
Chemistry - A European Journal, 2007 , vol. 13, # 12 p. 3354 - 3368
反应条件
lithium iodide in tetrahydrofuran; diethyl ether
T=50°C; Yield given;
参考文献
Concellon, Jose M.; Llavona, Lujan; Bernad, Pablo L. Jr.
Tetrahedron, 1995 , vol. 51, # 19 p. 5573 - 5584
