3-甲氧羰基苯硼酸频哪醇酯合成路线 （共 21 条）
反应条件
1: 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane With Pd(t-Bu3P)2; SPGS-550-M; NOK; potassium acetate in water Miyaura Borylation Reaction; 0.166667 h; Inert atmosphereSealed tube; 2: (3-bromophenyl)acetic acid methyl ester With SPGS-550-M; NOK in water 4 h; Inert atmosphereSealed tube; Reagent/catalyst;
参考文献
Journal of Organic Chemistry, , vol. 79, # 3 p. 888 - 900
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 2,2'-Bipyridine-4,4'-dicarboxylic acid in 2-methyl cyclohexane T=80°C; 12 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 50, # 45 p. 6176 - 6179
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 3 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6913 - 6917
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 2-(2-methoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; potassium acetate in 1,4-dioxane T=110°C; 24 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 7 p. 3543 - 3548
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in 1,4-dioxane T=20 - 90°C; 16 h;
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 18 p. 6234 - 6253
反应条件
Et3N; tetrabutylammonium iodide; 1,1'-bis-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) in 1,4-dioxane 100°C, 24 h; GC;
参考文献
Chemistry Letters, , vol. 40, # 9 p. 962 - 963
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I) in octane 80°C, 16 h, methylbenzoate (5.0 mmol), bis(pinacolato)diboron (1.0 mmol), (Ir(OMe)(COD))2 (0.015 mmol);
参考文献
Chemical Communications, , vol. 46, # 1 p. 159 - 161
反应条件
[Ir(OMe)(COD)]2/P(3,5-2F3C-C6H3)3 in octane 80°C, 16 h, methylbenzoate (5.0 mmol), bis(pinacolato)diboron (1.0 mmol), (Ir(OMe)(COD))2 (0.015 mmol), org. ligand (0.06 mmol);
参考文献
Chemical Communications, , vol. 46, # 1 p. 159 - 161
反应条件
in diphenylether T=170°C; 15 h;
参考文献
Tetrahedron, , vol. 64, # 5 p. 866 - 873
Chemical Communications, , # 31 p. 3323 - 3325
反应条件
in 1,2-dichloro-benzene T=180°C; 18 h;
参考文献
Tetrahedron, , vol. 64, # 5 p. 866 - 873
