1,4-二羟基-2-甲基萘合成路线 (共 60 条)
反应条件
sodium dithionite in diethyl ether; water
参考文献
Weerapreeyakul, Natthida; Visser, Petra; Brummelhuis, Mathijn; Gharat, Laxmikant; Chikhale, Prashant J.
Medicinal Chemistry Research, 2000 , vol. 10, # 3 p. 148 - 163
反应条件
in benzene T=120°C; 30 h;
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Ravichandran, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 233 - 235
反应条件
sulfuric acid; aluminium T=90°C;
参考文献
Eastman Kodak Co.
Patent: US2446519 , 1944 ;
Full Text Show Details
Eastman Kodak Co.
Patent: US2525515 , 1948 ;
反应条件
1: 93 percent / O2, salcomine / dimethylformamide / 2 h / Ambient temperature 2: 60 percent / benzene / 30 h / 120 °C View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Ravichandran, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 233 - 235
反应条件
1: 60 percent / ceric ammonium nitrate / acetonitrile; H2O / 12 h / Ambient temperature 2: 60 percent / benzene / 30 h / 120 °C View Scheme
参考文献
Rao, A. V. Rama; Deshpande, V. H.; Ravichandran, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 233 - 235
反应条件
triethylaluminum in benzene 25 h; Heating;
参考文献
Leal, J. M.; Arcos, J.; Garcia, B.
Zeitschrift fuer Physikalische Chemie (Leipzig), 1989 , vol. 270, # 5 p. 887 - 896
反应条件
pyridine hydrochloride
参考文献
Sah
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 1029,1034
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Pavolini
Ricerca Scientifica, 1958 , vol. 18, p. 134,137
Full Text Show Details
Jain; Seshadri
Proceedings - Indian Academy of Sciences, Section A, 1952 , vol. <A> 35, p. 233,238
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1.) THF, 5-15 deg C, sonication, 2 h, 2.) r.t., several hours; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Saa, Jose M.; Morey, Jeroni; Suner, Guillem; Frontera, Antoni; Costa, Antoni
Tetrahedron Letters, 1991 , vol. 32, # 49 p. 7313 - 7316
反应条件
1: tin (II)-chloride; glacial acetic acid 2: iron (III)-chloride; acetic acid 3: tin (II)-chloride; glacial acetic acid View Scheme
参考文献
Fries; Lohmann
Chemische Berichte, 1921 , vol. 54, p. 2917