1-苯基-1,3-丙二醇 合成路线 (共 84 条)
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
反应条件
lithium triethylborohydride in tetrahydrofuran
T=20°C; 2 h;
参考文献
Eames, Jason; Khanom, Hasina
Molecules, 2004 , vol. 9, # 5 p. 266 - 277
反应条件
sodium bis(2-methoxyethoxy)aluminium dihydride
Sharpless reaction;
参考文献
Mullah; Bentrude
Journal of Organic Chemistry, 1991 , vol. 56, # 26 p. 7218 - 7224
反应条件
lithium aluminium tetrahydride in diethyl ether
Ambient temperature;
参考文献
Ayer, William A.; Browne, Lois M.; Feng, Meow-Chen; Orszanska, Helena; Saeedi-Ghomi, Hossein
Canadian Journal of Chemistry, 1986 , vol. 64, p. 904 - 909
反应条件
sodium hydroxide; methanesulfonic acid; dihydrogen peroxide in tetrahydrofuran
T=65°C; 6 h;
参考文献
Brown, Herbert C.; Kim, Suk-Choong
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1064 - 1071
反应条件
potassium borohydride in ethanol
T=40°C; 4 h;
参考文献
Doussot, Joel; Guy, Alain; Garreau, Robert; Falguieres, Annie; Cossy, Janine; Amsterdamsky, Claude
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 2 p. 161 - 166
反应条件
sodium tetrahydroborate
T=20°C; 0.166667 h;
参考文献
Kim, Juryoung; De Castro, Kathlia A.; Lim, Minkyung; Rhee, Hakjune
Tetrahedron, 2010 , vol. 66, # 23 p. 3995 - 4001
反应条件
tetra-N-butylammonium borohydride in dichloromethane
Reduction; Heating;
参考文献
Narasimhan; Swarnalakshmi; Balakumar
Synthetic Communications, 2000 , vol. 30, # 5 p. 941 - 946
反应条件
lithium aluminium tetrahydride; diethyl ether
anschliessendes Behandeln mit Luft;
参考文献
Hochstein; Brown
Journal of the American Chemical Society, 1948 , vol. 70, p. 3484
反应条件
1: 56 percent / Ag2CO3 / Pd(OAc)2, PPh3 / dimethylformamide / 24 h / 60 °C
2: 95 percent / H2 / 5percent Pd-C / methanol
3: HCl
4: KOH / methanol
View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Tetrahedron Letters, 1992 , vol. 33, # 45 p. 6845 - 6848
反应条件
1: 95 percent / H2 / 5percent Pd-C / methanol
2: HCl
3: KOH / methanol
View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Yamanaka, Hiroshi
Tetrahedron Letters, 1992 , vol. 33, # 45 p. 6845 - 6848