1-苯基-1,4-丁二醇合成路线 （共 13 条）
反应条件
1: methanesulfonyl chloride / dichloromethane / 2 h / -10 °C 2: Wilkinson's catalyst / water; acetonitrile / 5 h / Inert atmosphere; Reflux View Scheme
参考文献
Periasamy, Mariappan; Sanjeevakumar, Nalluri; Dalai, Manasi; Gurubrahamam, Ramani; Reddy, Polimera Obula
Organic Letters, 2012 , vol. 14, # 12 p. 2932 - 2935
反应条件
cobalt(II) chloride in acetonitrile T=80°C; 3 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
cobalt(II) chloride in acetonitrile T=80°C; 4 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
1: 56 percent / Al2O3 2: 89 percent / imidazole / dimethylformamide 3: 86 percent / LiAlH4 / diethyl ether View Scheme
参考文献
Tamai, Yasufumi; Koike, Shinji; Ogura, Atsuhiko; Miyano, Sotaro
Journal of the Chemical Society, Chemical Communications, 1991 , # 12 p. 799 - 800
反应条件
indium(III) chloride; diphenylchlorosilane in 1,2-dichloro-ethane T=80°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 23 p. 7741 - 7744
反应条件
NH4BF4; sodium hydrogencarbonate; [{(η5-C5Me5)IrCl}2(μ-Cl)2] T=140°C; 17 h;
参考文献
Yamaguchi, Ryohei; Kawagoe, Shoko; Asai, Chiho; Fujita, Ken-Ichi
Organic Letters, 2008 , vol. 10, # 2 p. 181 - 184
反应条件
Oxonereg;; 2-iodo-3,4,5,6-tetramethylbenzoic acid in water; acetonitrile T=45°C; 15 h; Green chemistry;
参考文献
Tetrahedron, , vol. 70, # 13 p. 2286 - 2293
反应条件
pyridiniumchlorochromate on aluminumoxide T=20°C;
参考文献
Tetrahedron, , vol. 59, # 19 p. 3493 - 3498
反应条件
1: 56 percent / alumina / 24 h / Heating 2: 89 percent / imidazole / dimethylformamide / 3 h / 20 °C 3: 86 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 4: 52 percent / pyridine; DMAP / 2 h / 20 °C 5: 92 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 6: AcOH; H2O / tetrahydrofuran / 24 h / 40 °C View Scheme
参考文献
Tamai, Yasufumi; Hattori, Tetsutaro; Date, Masamitsu; Koike, Shinji; Kamikubo, Yoshinori; Akiyama, Masahiro; Seino, Kazuhiro; Takayama, Hideki; Oyama, Tomohito; Miyano, Sotaro
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1685 - 1694
反应条件
1: 56 percent / alumina / 24 h / Heating 2: 89 percent / imidazole / dimethylformamide / 3 h / 20 °C 3: 86 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 4: 52 percent / pyridine; DMAP / 2 h / 20 °C 5: 92 percent / LiAlH4 / diethyl ether / 1 h / 20 °C 6: AcOH; H2O / tetrahydrofuran / 24 h / 40 °C View Scheme
参考文献
Tamai, Yasufumi; Koike, Shinji; Ogura, Atsuhiko; Miyano, Sotaro
Journal of the Chemical Society, Chemical Communications, 1991 , # 12 p. 799 - 800
