反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209228', constants.ctx, '0')">formaldehyd</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br /> addn. of metal acetylacetonate into soln. of H2CO in H2O, heating to 60°C for 20 h under N2; removal of H2O and unreacted H2CO, product is trimethylsilylated and analyzed by GC; <br />
参考文献
Takeichi, Tsutomu; Sakurada, Yoshihiro; Hieda, Yoshihiro; Takayama, Yuzi Chemistry Letters, 1987 , p. 1301 - 1302