1,5-二苯基-1H-1,2,3-噻唑合成路线 （共 27 条）
反应条件
1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / |Inert atmosphere; |Schlenk technique
2: {Y[N(SiMe3)2]2(μ-Cl)(THF)}2 / tetrahydrofuran / 1 h / -78 °C / |Inert atmosphere; |Schlenk technique
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参考文献
Hong, Longcheng; Lin, Weijia; Zhang, Fangjun; Liu, Ruiting; Zhou, Xigeng
Chemical Communications, 2013 , vol. 49, # 49 p. 5589 - 5591
反应条件
1: ethanol / |Reflux
2: lithium tert-butylate; 4-toluenesulfonyl azide / dichloromethane / 20 °C
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参考文献
Cheng, Guolin; Zeng, Xiaobao; Shen, Jinhai; Wang, Xuesong; Cui, Xiuling
Angewandte Chemie - International Edition, 2013 , vol. 52, # 50 p. 13265 - 13268
Angew. Chem., 2013
反应条件
in benzene
T=70°C; 360 h;
参考文献
Cailleux, P.; Piet, J. C.; Benhaoua, H.; Carrie, R.
Bulletin des Societes Chimiques Belges, 1996 , vol. 105, # 1 p. 45 - 52
参考文献
Kirmse; Horner
Justus Liebigs Annalen der Chemie, 1958 , vol. 614, p. 1
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Moulin
Helvetica Chimica Acta, 1952 , vol. 35, p. 167,175
反应条件
sulfuric acid
1.) C6H6, 70 deg C, 24 h, 2.) RT, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Sakamoto, Takao; Uchiyama, Daishi; Kondo, Yoshinori; Yamanaka, Hiroshi
Heterocycles, 1993 , vol. 35, # 2 p. 1273 - 1278
参考文献
Kirmse; Horner
Justus Liebigs Annalen der Chemie, 1958 , vol. 614, p. 1
Full Text Show Details
Moulin
Helvetica Chimica Acta, 1952 , vol. 35, p. 167,175
参考文献
Dey, Santu; Datta, Dhrubajyoti; Pathak, Tanmaya
Synlett, 2011 , # 17 p. 2521 - 2524
